C₃₀H₄₄O₄

Base Information

Chemical Name:C₃₀H₄₄O₄
CAS No.:1375412-59-1
Molecular Formula:C₃₀H₄₄O₄
Molecular Weight:468.677
Hs Code.:

C<sub>30</sub>H<sub>44</sub>O<sub>4</sub>

Synonyms:

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Chemical Property of C₃₀H₄₄O₄

Chemical Property:

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Technology Process of C₃₀H₄₄O₄

There total 12 articles about C₃₀H₄₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 105-87-3,8022-83-1
3,7-dimethyl-2E,6-octadien-1-yl acetate

: 1375412-59-1
C₃₀H₄₄O₄

Guidance literature:: Multi-step reaction with 10 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 20 °C

2.1: dilithium tetrachlorocuprate / tetrahydrofuran / 1.5 h / 0 °C

3.1: sodium periodate / tetrahydrofuran; water / 7.5 h / 20 °C

4.1: sodium hydride / tetrahydrofuran; dimethyl sulfoxide; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

5.1: (1R,2R)-(-)-N,N'-bis(3,5-di-tert-butylsalicydene)-1,2-cyclohexanediaminocobalt(II); water; acetic acid / tetrahydrofuran / 17.5 h / 20 °C

6.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 - 20 °C

6.2: 1 h / -50 - -45 °C

6.3: 2 h / -70 - 0 °C

7.1: 2,6-dimethylpyridine; N-Bromosuccinimide; silver perchlorate / water; acetone / 0 - 0 h / 0 °C

8.1: samarium diiodide / tetrahydrofuran / 0.83 h / -20 °C

9.1: hydrogenchloride / methanol / 0.5 h / 20 °C

10.1: 2 h / 20 °C

With 2,6-dimethylpyridine; hydrogenchloride; sodium periodate; N-Bromosuccinimide; (1R,2R)-(-)-N,N'-bis(3,5-di-tert-butylsalicydene)-1,2-cyclohexanediaminocobalt(II); n-butyllithium; samarium diiodide; dilithium tetrachlorocuprate; water; silver perchlorate; sodium hydride; acetic acid; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; hexane; dichloromethane; water; dimethyl sulfoxide; acetone; mineral oil; 4.1: Corey-Chaykovsky reaction / 5.1: Jacobsen hydrolytic kinetic resolution / 6.3: Brook rearrangement / 8.1: Evans-Tishchenko reduction;
DOI:10.1002/anie.201108692

Reference yield:

: 1375412-52-4
C₃₃H₅₄O₂S₂Si

: 1375412-59-1
C₃₀H₄₄O₄

Guidance literature:: Multi-step reaction with 4 steps

1: 2,6-dimethylpyridine; N-Bromosuccinimide; silver perchlorate / water; acetone / 0 - 0 h / 0 °C

2: samarium diiodide / tetrahydrofuran / 0.83 h / -20 °C

3: hydrogenchloride / methanol / 0.5 h / 20 °C

4: 2 h / 20 °C

With 2,6-dimethylpyridine; hydrogenchloride; N-Bromosuccinimide; samarium diiodide; silver perchlorate; In tetrahydrofuran; methanol; water; acetone; 2: Evans-Tishchenko reduction;
DOI:10.1002/anie.201108692

Reference yield:

: 758692-16-9
(E)-2,2-dimethyl-3-(3-methyl-5-phenylpent-3-enyl)oxirane

: 1375412-59-1
C₃₀H₄₄O₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium periodate / tetrahydrofuran; water / 7.5 h / 20 °C

2.1: sodium hydride / tetrahydrofuran; dimethyl sulfoxide; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

3.1: (1R,2R)-(-)-N,N'-bis(3,5-di-tert-butylsalicydene)-1,2-cyclohexanediaminocobalt(II); water; acetic acid / tetrahydrofuran / 17.5 h / 20 °C

4.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 - 20 °C

4.2: 1 h / -50 - -45 °C

4.3: 2 h / -70 - 0 °C

5.1: 2,6-dimethylpyridine; N-Bromosuccinimide; silver perchlorate / water; acetone / 0 - 0 h / 0 °C

6.1: samarium diiodide / tetrahydrofuran / 0.83 h / -20 °C

7.1: hydrogenchloride / methanol / 0.5 h / 20 °C

8.1: 2 h / 20 °C

With 2,6-dimethylpyridine; hydrogenchloride; sodium periodate; N-Bromosuccinimide; (1R,2R)-(-)-N,N'-bis(3,5-di-tert-butylsalicydene)-1,2-cyclohexanediaminocobalt(II); n-butyllithium; samarium diiodide; water; silver perchlorate; sodium hydride; acetic acid; In tetrahydrofuran; methanol; hexane; water; dimethyl sulfoxide; acetone; mineral oil; 2.1: Corey-Chaykovsky reaction / 3.1: Jacobsen hydrolytic kinetic resolution / 4.3: Brook rearrangement / 6.1: Evans-Tishchenko reduction;
DOI:10.1002/anie.201108692