C₂₁H₃₁BrN₂O₄

Base Information

Chemical Name:C₂₁H₃₁BrN₂O₄
CAS No.:1393110-64-9
Molecular Formula:C₂₁H₃₁BrN₂O₄
Molecular Weight:455.392
Hs Code.:

C<sub>21</sub>H<sub>31</sub>BrN<sub>2</sub>O<sub>4</sub>

Synonyms:

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Chemical Property of C₂₁H₃₁BrN₂O₄

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Technology Process of C₂₁H₃₁BrN₂O₄

There total 8 articles about C₂₁H₃₁BrN₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3279-76-3,91914-07-7
6-hydroxy-2-methylpyridine

: 1393110-64-9
C₂₁H₃₁BrN₂O₄

: 1393110-66-1
C₂₁H₃₁BrN₂O₄

Guidance literature:: Multi-step reaction with 5 steps

1: silver carbonate / chloroform / 60 h

2: DBDMH / tetrahydrofuran / 72 h

3: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / Reflux

4: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; lithium diisopropyl amide / tetrahydrofuran / -50 - 10 °C

5: diethyl ether

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); silver carbonate; lithium diisopropyl amide; In tetrahydrofuran; tetrachloromethane; diethyl ether; chloroform;
DOI:10.1007/s11426-011-4480-y

Reference yield:

: 63071-03-4
2-methoxy-6-methyl-pyridine

: 1393110-64-9
C₂₁H₃₁BrN₂O₄

: 1393110-66-1
C₂₁H₃₁BrN₂O₄

Guidance literature:: Multi-step reaction with 4 steps

1: DBDMH / tetrahydrofuran / 72 h

2: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / Reflux

3: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; lithium diisopropyl amide / tetrahydrofuran / -50 - 10 °C

4: diethyl ether

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); lithium diisopropyl amide; In tetrahydrofuran; tetrachloromethane; diethyl ether;
DOI:10.1007/s11426-011-4480-y

Reference yield:

: 1393110-52-5
C₈H₉F₃O₄S

: 1393110-64-9
C₂₁H₃₁BrN₂O₄

: 1393110-66-1
C₂₁H₃₁BrN₂O₄

Guidance literature:: Multi-step reaction with 3 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; tert-butyl XPhos / toluene / 5 h / 80 °C

2: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; lithium diisopropyl amide / tetrahydrofuran / -50 - 10 °C

3: diethyl ether

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; lithium diisopropyl amide; tert-butyl XPhos; In tetrahydrofuran; diethyl ether; toluene; 1: Buchwald-Hartwig coupling;
DOI:10.1007/s11426-011-4480-y