Technology Process of C32H28ClNO2S
There total 11 articles about C32H28ClNO2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / acetone / Reflux
2: sodium hydrogen sulfide; magnesium chloride / N,N-dimethyl-formamide / 20 °C
3: ethanol / Reflux
With
sodium hydrogen sulfide; potassium carbonate; magnesium chloride;
In
ethanol; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.bmcl.2012.10.022
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium hydroxide / methanol / Reflux
2: thionyl chloride / Reflux
3: triethylamine / dichloromethane / 0 °C
4: tetrahydrofuran / -78 °C
5: sulfuryl dichloride / dichloromethane / -10 °C
6: ethanol / Reflux
With
thionyl chloride; sulfuryl dichloride; triethylamine; sodium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2012.10.022
- Guidance literature:
-
Multi-step reaction with 7 steps
1: copper(I) oxide; caesium carbonate / N,N-dimethyl-formamide / 110 °C / Molecular sieve
2: sodium hydroxide / methanol / Reflux
3: thionyl chloride / Reflux
4: triethylamine / dichloromethane / 0 °C
5: tetrahydrofuran / -78 °C
6: sulfuryl dichloride / dichloromethane / -10 °C
7: ethanol / Reflux
With
copper(I) oxide; thionyl chloride; sulfuryl dichloride; caesium carbonate; triethylamine; sodium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.10.022