2-<(3S,5R,6R)-3,5,6-trihydroxy-5,6-dihydro-β-ionyliden>acetaldehyd

Base Information

Chemical Name:2-<(3S,5R,6R)-3,5,6-trihydroxy-5,6-dihydro-β-ionyliden>acetaldehyd
CAS No.:96140-14-6
Molecular Formula:C₁₇H₂₆O₅
Molecular Weight:310.39
Hs Code.:

Synonyms:

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Chemical Property of 2-<(3S,5R,6R)-3,5,6-trihydroxy-5,6-dihydro-β-ionyliden>acetaldehyd

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Technology Process of 2-<(3S,5R,6R)-3,5,6-trihydroxy-5,6-dihydro-β-ionyliden>acetaldehyd

There total 8 articles about 2-<(3S,5R,6R)-3,5,6-trihydroxy-5,6-dihydro-β-ionyliden>acetaldehyd which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54165-55-8
(3R)-3-Acetoxy-β-ionon

: 96140-14-6
2-<(3S,5R,6R)-3,5,6-trihydroxy-5,6-dihydro-β-ionyliden>acetaldehyd

Guidance literature:: Multi-step reaction with 5 steps

1: m-chloroperbenzoic acid / CHCl₃ / 0 deg C, 5 h; RT, 20 h

2: 93 percent / NaH / hexane; tetrahydrofuran / 20 h / Ambient temperature

3: 83 percent / H₂SO₄ / tetrahydrofuran; H₂O / RT, 30 min; 50 deg C, 2.5 h

4: 76 percent / DIBAH / diethyl ether; hexane / 1.5 h / 0 °C

5: MnO₂ / ethyl acetate / 1 h / Ambient temperature

With manganese(IV) oxide; sulfuric acid; sodium hydride; diisobutylaluminium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; hexane; chloroform; water; ethyl acetate;
DOI:10.1002/hlca.19840670804

Reference yield:

: 50281-40-8
(3S,5S,6R)-3-acetoxy-5,6-epoxy-5,6-dihydro-β-ionon

: 96140-14-6
2-<(3S,5R,6R)-3,5,6-trihydroxy-5,6-dihydro-β-ionyliden>acetaldehyd

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / NaH / hexane; tetrahydrofuran / 20 h / Ambient temperature

2: 83 percent / H₂SO₄ / tetrahydrofuran; H₂O / RT, 30 min; 50 deg C, 2.5 h

3: 76 percent / DIBAH / diethyl ether; hexane / 1.5 h / 0 °C

4: MnO₂ / ethyl acetate / 1 h / Ambient temperature

With manganese(IV) oxide; sulfuric acid; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; diethyl ether; hexane; water; ethyl acetate;
DOI:10.1002/hlca.19840670804