11H-Benzo[b]fluoren-11-one, 4,5,9,10-tetramethoxy-2-methyl-

Base Information

Chemical Name:11H-Benzo[b]fluoren-11-one, 4,5,9,10-tetramethoxy-2-methyl-
CAS No.:133129-36-9
Molecular Formula:C22H20O5
Molecular Weight:364.398
Hs Code.:
DSSTox Substance ID:DTXSID10454070
Nikkaji Number:J817.408C
Wikidata:Q82275403

Synonyms:133129-36-9;11H-Benzo[b]fluoren-11-one, 4,5,9,10-tetramethoxy-2-methyl-;DTXSID10454070;2-Methyl-4,5,9,10-tetramethoxy-11H-benzo[b]fluoren-11-one

Suppliers and Price of 11H-Benzo[b]fluoren-11-one, 4,5,9,10-tetramethoxy-2-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 11H-Benzo[b]fluoren-11-one, 4,5,9,10-tetramethoxy-2-methyl-

Chemical Property:

XLogP3:4.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:364.13107373
Heavy Atom Count:27
Complexity:551

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=C(C(=C1)OC)C3=C(C4=C(C(=CC=C4)OC)C(=C3C2=O)OC)OC

Technology Process of 11H-Benzo[b]fluoren-11-one, 4,5,9,10-tetramethoxy-2-methyl-

There total 2 articles about 11H-Benzo[b]fluoren-11-one, 4,5,9,10-tetramethoxy-2-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 133129-33-6
1,4,8-trimethoxy-3-(2-bromo-4-methyl-6-methoxyphenyl)naphthalene-2-carboxamide

: 133129-36-9
tri-O-methylkinafluorenone

: 139976-11-7
1,4,8-trimethoxy-3-(2-methoxy-4-methylphenyl)naphthalene-2-carboxamide

: 133129-34-7
1,4,8-trimethoxy-3-(2-methoxy-6-formyl-4-methylphenyl)naphthalene-2-carboxamide

Guidance literature:: With tert.-butyl lithium; N,N-dimethyl-formamide; Yield given. Multistep reaction. Yields of byproduct given; 1) -98 deg C;
DOI:10.1021/jo00007a009

Reference yield:

: 133129-33-6
1,4,8-trimethoxy-3-(2-bromo-4-methyl-6-methoxyphenyl)naphthalene-2-carboxamide

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 133129-36-9
tri-O-methylkinafluorenone

: 139976-11-7
1,4,8-trimethoxy-3-(2-methoxy-4-methylphenyl)naphthalene-2-carboxamide

: 133129-34-7
1,4,8-trimethoxy-3-(2-methoxy-6-formyl-4-methylphenyl)naphthalene-2-carboxamide

Guidance literature:: With tert.-butyl lithium; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, pentane, -98 deg C, 1 h, 2a.) -78 deg C, 0.5 h, 2b.) 0 deg C, 0.5 h;
DOI:10.1021/jo00036a005