Technology Process of C13H9(18)FO2
There total 2 articles about C13H9(18)FO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
(5-(tert-butyl)-2-hydroxyphenyl)(phenyl)methanone;
With
[18F]-tetrabutylammonium fluoride; [bis(acetoxy)iodo]benzene; trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 0.25h;
With
trifluoroacetic acid;
In
dichloromethane;
for 0.166667h;
DOI:10.1002/anie.201201502
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: bis(benzonitrile)palladium(II) dichloride; oxygen; sodium hydrogencarbonate; copper dichloride / N,N-dimethyl-formamide / 14 h / 80 °C
2.1: [18F]-tetrabutylammonium fluoride; [bis(acetoxy)iodo]benzene; trifluoroacetic acid / dichloromethane / 0.25 h / 20 °C
2.2: 0.17 h
With
bis(benzonitrile)palladium(II) dichloride; [18F]-tetrabutylammonium fluoride; [bis(acetoxy)iodo]benzene; oxygen; sodium hydrogencarbonate; trifluoroacetic acid; copper dichloride;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201201502