C₅₂H₂₆N₄Zn

Base Information

Chemical Name:C₅₂H₂₆N₄Zn
CAS No.:1361989-40-3
Molecular Formula:C₅₂H₂₆N₄Zn
Molecular Weight:772.195
Hs Code.:

C<sub>52</sub>H<sub>26</sub>N<sub>4</sub>Zn

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₂H₂₆N₄Zn

Chemical Property:

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Technology Process of C₅₂H₂₆N₄Zn

There total 5 articles about C₅₂H₂₆N₄Zn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1361989-37-8
C₅₂H₂₈N₄Zn

: 1361989-40-3
C₅₂H₂₆N₄Zn

Guidance literature:: With toluene; at 110 ℃; for 2h;
DOI:10.1002/chem.201102488

Reference yield:

: 917-23-7,20998-75-8
5,15,10,20-tetraphenylporphyrin

: 1361989-40-3
C₅₂H₂₆N₄Zn

Guidance literature:: Multi-step reaction with 5 steps

1: N-Bromosuccinimide / chloroform / 24 h / Reflux

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 6 h / 80 °C / Inert atmosphere

3: zinc acetate hydrate / methanol; chloroform / 1 h / 20 °C

4: tetrabutyl ammonium fluoride / tetrahydrofuran

5: toluene / 2 h / 110 °C

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; zinc acetate hydrate; tetrabutyl ammonium fluoride; toluene; In tetrahydrofuran; methanol; chloroform; 5: Bergmann reaction;
DOI:10.1002/chem.201102488

Reference yield:

: 2,3,12,13-tetrakis(trimethylsilylethynyl)-5,10,15,20-tetraphenylporphyrin

: 1361989-40-3
C₅₂H₂₆N₄Zn

Guidance literature:: Multi-step reaction with 3 steps

1: zinc acetate hydrate / methanol; chloroform / 1 h / 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran

3: toluene / 2 h / 110 °C

With zinc acetate hydrate; tetrabutyl ammonium fluoride; toluene; In tetrahydrofuran; methanol; chloroform; 3: Bergmann reaction;
DOI:10.1002/chem.201102488