C₁₉H₂₁NS

Base Information

Chemical Name:C₁₉H₂₁NS
CAS No.:77228-94-5
Molecular Formula:C₁₉H₂₁NS
Molecular Weight:295.448
Hs Code.:

Synonyms:

Suppliers and Price of C₁₉H₂₁NS

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₉H₂₁NS

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₉H₂₁NS

There total 7 articles about C₁₉H₂₁NS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 77243-08-4
4-((1S,3S,4S,5S,6R)-2-Chloromethyl-3-methyl-5-phenylsulfanyl-tricyclo[2.2.1.0^2,6]hept-3-yl)-butyronitrile

: 77228-94-5,77286-00-1
C₁₉H₂₁NS

Guidance literature:: With lithium diethylamide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 ℃;
DOI:10.1016/0040-4039(80)88100-7

Reference yield:

: 73565-76-1
(1R,2S,4S)-2-Methyl-3-methylene-bicyclo[2.2.1]hept-5-ene-2-carbaldehyde

: 77228-94-5,77286-00-1
C₁₉H₂₁NS

Guidance literature:: Multi-step reaction with 6 steps

1: dimethylsulfoxide / Ambient temperature

2: acidic silica gel / CH₂Cl₂ / 48 h

3: 92 percent / CH₃S(O)CH₂Na / dimethylsulfoxide / Horner-Emmons reaction

4: 96 percent / Mg / methanol

5: 100 percent / CH₂Cl₂ / 0 °C

6: 81 percent / LiN(C₂H₅)2 / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 °C

With lithium diethylamide; silica gel; sodium methylsulfinylmethanide; magnesium; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; dimethyl sulfoxide;
DOI:10.1016/0040-4039(80)88100-7

Reference yield:

: 77228-96-7
((1R,2S,4S)-2-Methyl-3-methylene-bicyclo[2.2.1]hept-5-en-2-yl)-acetaldehyde

: 77228-94-5,77286-00-1
C₁₉H₂₁NS

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / CH₃S(O)CH₂Na / dimethylsulfoxide / Horner-Emmons reaction

2: 96 percent / Mg / methanol

3: 100 percent / CH₂Cl₂ / 0 °C

4: 81 percent / LiN(C₂H₅)2 / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 °C

With lithium diethylamide; sodium methylsulfinylmethanide; magnesium; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; dimethyl sulfoxide;
DOI:10.1016/0040-4039(80)88100-7