C₃₇H₅₁NO₁₁

Base Information

Chemical Name:C₃₇H₅₁NO₁₁
CAS No.:1352816-16-0
Molecular Formula:C₃₇H₅₁NO₁₁
Molecular Weight:685.812
Hs Code.:

C<sub>37</sub>H<sub>51</sub>NO<sub>11</sub>

Synonyms:

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Chemical Property of C₃₇H₅₁NO₁₁

Chemical Property:

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Technology Process of C₃₇H₅₁NO₁₁

There total 14 articles about C₃₇H₅₁NO₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₆H₄₇NO₁₁

: 544-97-8
dimethyl zinc(II)

: 1352816-16-0
C₃₇H₅₁NO₁₁

: C₃₇H₅₁NO₁₁

Guidance literature:: dimethyl zinc(II); With copper(I) trifluoromethanesolfonate toluene complex; N-[2-(diphenylphosphino)benzylidene]-L-Tle-L-Tyr(OBn)-NEt₂; In toluene; at -30 ℃; for 0.166667h; Inert atmosphere;

C₃₆H₄₇NO₁₁; In toluene; at -30 - 0 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.1002/anie.201104681

Reference yield:

: 1352816-12-6
C₃₃H₄₄O₉

: 1352816-16-0
C₃₇H₅₁NO₁₁

: C₃₇H₅₁NO₁₁

Guidance literature:: Multi-step reaction with 6 steps

1.1: dichloromethane / 1.5 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

4.1: Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C

5.1: ammonium acetate; sodium sulfate / 19 h / 75 °C

6.1: copper(I) trifluoromethanesolfonate toluene complex; N-[2-(diphenylphosphino)benzylidene]-L-Tle-L-Tyr(OBn)-NEt₂ / toluene / 0.17 h / -30 °C / Inert atmosphere

6.2: -30 - 0 °C / Inert atmosphere

With copper(I) trifluoromethanesolfonate toluene complex; N-[2-(diphenylphosphino)benzylidene]-L-Tle-L-Tyr(OBn)-NEt₂; ammonium acetate; tetrabutyl ammonium fluoride; Dess-Martin periodane; sodium sulfate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1002/anie.201104681

Reference yield:

: 1352816-07-9
C₅₀H₆₄O₈Si

: 1352816-16-0
C₃₇H₅₁NO₁₁

: C₃₇H₅₁NO₁₁

Guidance literature:: Multi-step reaction with 13 steps

1.1: o-xylene / 20 h / 165 °C / Inert atmosphere

2.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C

2.2: NaBO₃*4H₂O / 3 h / 20 °C

3.1: pyridine; dmap / dichloromethane / 1 h / 0 - 20 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 20 °C

5.1: pyridine; tributylphosphine / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere

6.1: dihydrogen peroxide / dichloromethane; water / 29 h / 20 °C / pH 7 / aq. phosphate buffer

7.1: cerium(III) chloride heptahydrate; oxalic acid / acetonitrile / 2 h / 20 °C

8.1: dichloromethane / 1.5 h / 20 °C

9.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

11.1: Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C

12.1: ammonium acetate; sodium sulfate / 19 h / 75 °C

13.1: copper(I) trifluoromethanesolfonate toluene complex; N-[2-(diphenylphosphino)benzylidene]-L-Tle-L-Tyr(OBn)-NEt₂ / toluene / 0.17 h / -30 °C / Inert atmosphere

13.2: -30 - 0 °C / Inert atmosphere

With pyridine; dmap; copper(I) trifluoromethanesolfonate toluene complex; tributylphosphine; cerium(III) chloride heptahydrate; N-[2-(diphenylphosphino)benzylidene]-L-Tle-L-Tyr(OBn)-NEt₂; ammonium acetate; tetrabutyl ammonium fluoride; dihydrogen peroxide; oxalic acid; Dess-Martin periodane; sodium sulfate; N-ethyl-N,N-diisopropylamine; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; dichloromethane; o-xylene; water; toluene; acetonitrile; 2.1: Hydroboration reaction;
DOI:10.1002/anie.201104681