Technology Process of C41H33ClO5
There total 6 articles about C41H33ClO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C28H23ClO4; C21H12B3F9O12S3;
With
potassium fluoride; tris-(dibenzylideneacetone)dipalladium(0); tri tert-butylphosphoniumtetrafluoroborate;
In
tetrahydrofuran; water;
at 50 ℃;
for 22h;
Inert atmosphere;
5-chloro-1,3-dihydro-2,1-benzoxaborol-1-ol;
With
1,1'-bis-(diphenylphosphino)ferrocene; potassium fluoride; palladium diacetate;
In
tetrahydrofuran;
at 50 ℃;
for 22h;
chemoselective reaction;
Inert atmosphere;
DOI:10.1021/ol200676k
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 1,1'-bis-(diphenylphosphino)ferrocene; potassium fluoride; palladium diacetate / tetrahydrofuran / 22 h / 50 °C / Inert atmosphere
2.1: tris-(dibenzylideneacetone)dipalladium(0); potassium fluoride; tri tert-butylphosphoniumtetrafluoroborate / tetrahydrofuran; water / 22 h / 50 °C / Inert atmosphere
2.2: 22 h / 50 °C / Inert atmosphere
With
1,1'-bis-(diphenylphosphino)ferrocene; potassium fluoride; tris-(dibenzylideneacetone)dipalladium(0); palladium diacetate; tri tert-butylphosphoniumtetrafluoroborate;
In
tetrahydrofuran; water;
1.1: Suzuki-Miyaura coupling / 2.1: Suzuki-Miyaura coupling;
DOI:10.1021/ol200676k
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tris-(dibenzylideneacetone)dipalladium(0); potassium phosphate; tri tert-butylphosphoniumtetrafluoroborate / tetrahydrofuran; water / 22 h / 50 °C / Inert atmosphere
2.1: 1,1'-bis-(diphenylphosphino)ferrocene; potassium fluoride; palladium diacetate / tetrahydrofuran / 22 h / 50 °C / Inert atmosphere
3.1: tris-(dibenzylideneacetone)dipalladium(0); potassium fluoride; tri tert-butylphosphoniumtetrafluoroborate / tetrahydrofuran; water / 22 h / 50 °C / Inert atmosphere
3.2: 22 h / 50 °C / Inert atmosphere
With
1,1'-bis-(diphenylphosphino)ferrocene; potassium fluoride; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); palladium diacetate; tri tert-butylphosphoniumtetrafluoroborate;
In
tetrahydrofuran; water;
1.1: Suzuki-Miyaura coupling / 2.1: Suzuki-Miyaura coupling / 3.1: Suzuki-Miyaura coupling;
DOI:10.1021/ol200676k