6-benzyl-2,2-diethoxy-1,3,6,2-dioxazagermocane

Base Information

Chemical Name:6-benzyl-2,2-diethoxy-1,3,6,2-dioxazagermocane
CAS No.:1207181-40-5
Molecular Formula:C₁₅H₂₅GeNO₄
Molecular Weight:355.958
Hs Code.:

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Chemical Property of 6-benzyl-2,2-diethoxy-1,3,6,2-dioxazagermocane

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Technology Process of 6-benzyl-2,2-diethoxy-1,3,6,2-dioxazagermocane

There total 2 articles about 6-benzyl-2,2-diethoxy-1,3,6,2-dioxazagermocane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 101-32-6
N-benzyl-diethanolamine

: 14165-55-0
tetraethoxygermanium

: 1207181-40-5
6-benzyl-2,2-diethoxy-1,3,6,2-dioxazagermocane

Guidance literature:: In benzene; byproducts: C2H5OH; under Ar, Schlenk technique; soln. of Ge(OEt)4 (1 equiv.) and PhCH2N(CH2CH2OH)2 (1 equiv.) in C6H6 refluxed for 5 h; evapn. under vac., residue washed with ether; elem. anal.;
DOI:10.1134/S0036023609020077

Reference yield: 63.0%

: 1220910-67-7
6-benzyl-2-(4-methylphenyl)-1,3,6,2-dioxazaborocane

: 14165-55-0
tetraethoxygermanium

: 1207181-40-5
6-benzyl-2,2-diethoxy-1,3,6,2-dioxazagermocane

Guidance literature:: With AlCl₃; In toluene; Ge(OEt)4 and AlCl3 were added to soln. of borocane, mixt. was refluxed for 6 h; volatiles were removed in vac., residue was washed with Et2O, dried in vac.; NMR;
DOI:10.1007/s11172-008-0259-5