Thiocyanic acid, diphenylmethyl ester

Base Information

• Chemical Name: Thiocyanic acid, diphenylmethyl ester
• CAS No.: 13317-56-1
• Molecular Formula: C14H11NS
• Molecular Weight: 225.314

Synonyms:

Chemical Property of Thiocyanic acid, diphenylmethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Thiocyanic acid, diphenylmethyl ester

There total 21 articles about Thiocyanic acid, diphenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1,1-Diphenylmethanol (91-01-0) + ammonium thiocyanate (1147550-11-5) → (thiocyanato)(diphenyl)methane (13317-56-1)

Guidance literature:

niobium pentachloride; In acetonitrile; at 20 ℃; for 0.5h;

DOI:10.1016/j.tetlet.2007.09.140

Reference yield: 88.0%

1,1-Diphenylmethanol (91-01-0) + ammonium thiocyanate (1147550-11-5) → (thiocyanato)(diphenyl)methane (13317-56-1) + diphenylmethyl isothiocyanate (3550-21-8)

Guidance literature:

With bromine; triphenylphosphine; In acetonitrile; at 20 ℃;

DOI:10.1039/a906113d

Reference yield: 80.0%

Diphenylmethane (101-81-5) + N-selenocyanatosaccharin → (thiocyanato)(diphenyl)methane (13317-56-1)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); In benzene; at 80 ℃; for 4h;

DOI:10.1039/d1cc04302a

upstream raw materials:

thiocyanogen

Diphenylmethane

diphenylmethyl isothiocyanate

potassium thioacyanate

Downstream raw materials:

diphenylmethyl isothiocyanate

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