4'-(4-carboxyphenyl)-2,2':6',2''-terpyridine(1,10-phenanthroline)chloride ruthenium(II) tetrafluoroborate

Base Information

Chemical Name:4'-(4-carboxyphenyl)-2,2':6',2''-terpyridine(1,10-phenanthroline)chloride ruthenium(II) tetrafluoroborate
CAS No.:1352132-23-0
Molecular Formula:BF₄*C₃₄H₂₃ClN₅O₂Ru
Molecular Weight:756.917
Hs Code.:

Synonyms:

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Chemical Property of 4'-(4-carboxyphenyl)-2,2':6',2''-terpyridine(1,10-phenanthroline)chloride ruthenium(II) tetrafluoroborate

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Technology Process of 4'-(4-carboxyphenyl)-2,2':6',2''-terpyridine(1,10-phenanthroline)chloride ruthenium(II) tetrafluoroborate

There total 1 articles about 4'-(4-carboxyphenyl)-2,2':6',2''-terpyridine(1,10-phenanthroline)chloride ruthenium(II) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 13755-29-8
sodium tetrafluoroborate

: 66-71-7
1,10-Phenanthroline

: 637740-33-1
trichloro(4-(4-carboxyphenyl)-2,2':6,2''-terpyridine)ruthenium(III)

: 1352132-23-0
4'-(4-carboxyphenyl)-2,2':6',2''-terpyridine(1,10-phenanthroline)chloride ruthenium(II) tetrafluoroborate

Guidance literature:: In methanol; ethanol; soln. of complex and ligand (1:1 mol) in EtOH refluxed for 10 h with stirring; vol. reduced; methanolic soln. of NaBF4 added; product filtered off; washed (H2O, EtOH); dried (vac.); chromy. (SiO2, MeCN:aq. satd. soln. KNO3:H2O = 14:2:1); aq. soln. of NaBF4 added; ppt. filtered; washed (H2O, EtOH, Et2O); crystd. (MeCN/H2O); elem. anal.;
DOI:10.1016/j.poly.2011.09.014