2-amino-4-(4-chlorophenyl)-3-cyclobutylmethoxybutane

Base Information

Chemical Name:2-amino-4-(4-chlorophenyl)-3-cyclobutylmethoxybutane
CAS No.:605680-65-7
Molecular Formula:C₁₅H₂₂ClNO
Molecular Weight:267.799
Hs Code.:

Synonyms:

Suppliers and Price of 2-amino-4-(4-chlorophenyl)-3-cyclobutylmethoxybutane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-amino-4-(4-chlorophenyl)-3-cyclobutylmethoxybutane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-amino-4-(4-chlorophenyl)-3-cyclobutylmethoxybutane

There total 5 articles about 2-amino-4-(4-chlorophenyl)-3-cyclobutylmethoxybutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 605680-66-8
methyl 2-diazo-3(4-chlorophenyl)propanoate

: 605680-65-7
2-amino-4-(4-chlorophenyl)-3-cyclobutylmethoxybutane

Guidance literature:: Multi-step reaction with 4 steps

1.1: dirhodium tetraacetate / benzene / 1.5 h / 90 °C

2.1: dimethylaluminum chloride / hexane; dichloromethane / 1 h / 0 - 20 °C

2.2: 20 °C

3.1: tetrahydrofuran; diethyl ether / 4 h / 0 - 20 °C

4.1: ammonium acetate; sodium cyanoborohydride / dichloromethane / 20 °C

4.2: 0.5 h

With ammonium acetate; dimethylaluminum chloride; sodium cyanoborohydride; dirhodium tetraacetate; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; benzene;

Reference yield:

: 15028-44-1
DL-phenylalanine methyl ester

: 605680-65-7
2-amino-4-(4-chlorophenyl)-3-cyclobutylmethoxybutane

Guidance literature:: Multi-step reaction with 5 steps

1.1: acetic acid; isopentyl nitrite / chloroform / 0.5 h / 0 - 73 °C

2.1: dirhodium tetraacetate / benzene / 1.5 h / 90 °C

3.1: dimethylaluminum chloride / hexane; dichloromethane / 1 h / 0 - 20 °C

3.2: 20 °C

4.1: tetrahydrofuran; diethyl ether / 4 h / 0 - 20 °C

5.1: ammonium acetate; sodium cyanoborohydride / dichloromethane / 20 °C

5.2: 0.5 h

With ammonium acetate; dimethylaluminum chloride; sodium cyanoborohydride; acetic acid; isopentyl nitrite; dirhodium tetraacetate; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; chloroform; benzene;

Reference yield:

: 4415-82-1
cyclobutanemethanol

: 605680-65-7
2-amino-4-(4-chlorophenyl)-3-cyclobutylmethoxybutane

Guidance literature:: Multi-step reaction with 4 steps

1.1: dirhodium tetraacetate / benzene / 1.5 h / 90 °C

2.1: dimethylaluminum chloride / hexane; dichloromethane / 1 h / 0 - 20 °C

2.2: 20 °C

3.1: tetrahydrofuran; diethyl ether / 4 h / 0 - 20 °C

4.1: ammonium acetate; sodium cyanoborohydride / dichloromethane / 20 °C

4.2: 0.5 h

With ammonium acetate; dimethylaluminum chloride; sodium cyanoborohydride; dirhodium tetraacetate; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; benzene;