(5S,11S,13aR)-5-Benzyl-11-((R)-6-hydroxy-6-(S)-oxiranyl-hexyl)-8,8-dimethyl-decahydro-3a,6,9,12-tetraaza-cyclopentacyclododecene-4,7,10,13-tetraone

Base Information

Chemical Name:(5S,11S,13aR)-5-Benzyl-11-((R)-6-hydroxy-6-(S)-oxiranyl-hexyl)-8,8-dimethyl-decahydro-3a,6,9,12-tetraaza-cyclopentacyclododecene-4,7,10,13-tetraone
CAS No.:107982-60-5
Molecular Formula:C₂₈H₄₀N₄O₆
Molecular Weight:528.649
Hs Code.:

(5S,11S,13aR)-5-Benzyl-11-((R)-6-hydroxy-6-(S)-oxiranyl-hexyl)-8,8-dimethyl-decahydro-3a,6,9,12-tetraaza-cyclopentacyclododecene-4,7,10,13-tetraone

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Chemical Property of (5S,11S,13aR)-5-Benzyl-11-((R)-6-hydroxy-6-(S)-oxiranyl-hexyl)-8,8-dimethyl-decahydro-3a,6,9,12-tetraaza-cyclopentacyclododecene-4,7,10,13-tetraone

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Technology Process of (5S,11S,13aR)-5-Benzyl-11-((R)-6-hydroxy-6-(S)-oxiranyl-hexyl)-8,8-dimethyl-decahydro-3a,6,9,12-tetraaza-cyclopentacyclododecene-4,7,10,13-tetraone

There total 28 articles about (5S,11S,13aR)-5-Benzyl-11-((R)-6-hydroxy-6-(S)-oxiranyl-hexyl)-8,8-dimethyl-decahydro-3a,6,9,12-tetraaza-cyclopentacyclododecene-4,7,10,13-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 52574-64-8,107982-60-5,107982-61-6,108146-59-4
(5S,11S,13aR)-5-Benzyl-11-((R)-6-hydroxy-6-(S)-oxiranyl-hexyl)-8,8-dimethyl-decahydro-3a,6,9,12-tetraaza-cyclopentacyclododecene-4,7,10,13-tetraone

Guidance literature:: With titanium(IV) isopropylate; tert.-butylhydroperoxide; (-)-diisopropyl tartrate; In dichloromethane;
DOI:10.1016/S0040-4039(00)84399-3

Reference yield: 24.0%

: 52574-64-8,107982-60-5,107982-61-6,108146-59-4
(5S,11S,13aR)-5-Benzyl-11-((S)-6-hydroxy-6-(R)-oxiranyl-hexyl)-8,8-dimethyl-decahydro-3a,6,9,12-tetraaza-cyclopentacyclododecene-4,7,10,13-tetraone

Guidance literature:: With titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; In dichloromethane;
DOI:10.1016/S0040-4039(00)84399-3

Reference yield:

: 108071-98-3
Methyl of N-<2(S)-benzyloxycarbonylamino-10-chloro-8(S),9(R)-O-isopropylidenedecanoyl>-dimethylglycyl-(S)-phenylalanyl-(R)-prolinate

: 52574-64-8,107982-60-5,107982-61-6,108146-59-4
Dihydrochlamydocin

Guidance literature:: Multi-step reaction with 4 steps

1: NaOH / H₂O; dioxane / 5 h / Ambient temperature

2: DCCD / ethyl acetate / -20 deg C to RT

3: 94 percent / H₂ / Pd / dioxane / 5 h / 95 °C

4: 1.) HOOC-COOH 2.) K₂CO₃ / 1.) dioxane/H₂O, 80 deg C, 4 h 2.) MeOH, RT, 4 h

With sodium hydroxide; hydrogen; oxalic acid; potassium carbonate; dicyclohexyl-carbodiimide; palladium; In 1,4-dioxane; water; ethyl acetate;