1,4-(bis-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolane-2-yl)phenyl]-amino)-phenyl ethanol

Base Information

Chemical Name:1,4-(bis-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolane-2-yl)phenyl]-amino)-phenyl ethanol
CAS No.:376363-37-0
Molecular Formula:C₃₂H₄₁B₂NO₅
Molecular Weight:541.303
Hs Code.:

Synonyms:

Suppliers and Price of 1,4-(bis-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolane-2-yl)phenyl]-amino)-phenyl ethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,4-(bis-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolane-2-yl)phenyl]-amino)-phenyl ethanol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,4-(bis-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolane-2-yl)phenyl]-amino)-phenyl ethanol

There total 1 articles about 1,4-(bis-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolane-2-yl)phenyl]-amino)-phenyl ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.8%

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 121-43-7,63156-11-6
Trimethyl borate

: 98311-81-0
1-(4-[bis-(4-bromophenyl)-amino]-phenyl)ethanol

: 376363-37-0
1,4-(bis-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolane-2-yl)phenyl]-amino)-phenyl ethanol

Guidance literature:: With n-butyllithium; In diethyl ether; sol. of 1-(4-(bis-(4-bromophenyl)-amino)-phenyl)ethanol cooled to -78°C; stirred; n-BuLi added dropwise; after 2 h sol. warmed gently to room temp.; cooled to -78°C; (CH3O)3B added; stirred, 2 h; warmedto room temp.; sol. of pinacol added; washed (water); sepd.; dried (MgSO4); solvent evapd.; column chromy. (diethyl ether/petroleum ether);
DOI:10.1016/S0013-4686(01)00535-7

Reference yield: 33.0%

: 376363-37-0
1,4-(bis-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolane-2-yl)phenyl]-amino)-phenyl ethanol

: 376363-34-7
bis-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolane-2-yl)phenyl]-(4-vinylphenyl) amine

Guidance literature:: With trichlorophosphate; In pyridine; (Ar); sol. heated under reflux for more than 12 h; thin-layer chromy.; cooled to room temp.; extd. (water/diethyl ether); treated with ethyl acetate, then dichloromethane; dried (MgSO4); solvent evapd.; chromy. (diethyl ether/petroleum ether);
DOI:10.1016/S0013-4686(01)00535-7