Technology Process of C20H27BrN2O3S
There total 6 articles about C20H27BrN2O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / -20 °C
1.2: -20 °C
2.1: hydrogenchloride / diethyl ether / -20 °C
3.1: lithium tri-t-butoxyaluminum hydride / ethanol / -78 °C
4.1: isopropyl alcohol / 70 °C
5.1: sodium hydrogencarbonate / water; 1,2-dichloro-ethane
6.1: 10% palladium on activated charcoal; ammonium formate / methanol
With
4-methyl-morpholine; hydrogenchloride; 10% palladium on activated charcoal; ammonium formate; sodium hydrogencarbonate; lithium tri-t-butoxyaluminum hydride; isobutyl chloroformate;
In
tetrahydrofuran; methanol; diethyl ether; ethanol; water; 1,2-dichloro-ethane; isopropyl alcohol;
DOI:10.1111/j.1747-0285.2010.00995.x
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogenchloride / diethyl ether / -20 °C
2: lithium tri-t-butoxyaluminum hydride / ethanol / -78 °C
3: isopropyl alcohol / 70 °C
4: sodium hydrogencarbonate / water; 1,2-dichloro-ethane
5: 10% palladium on activated charcoal; ammonium formate / methanol
With
hydrogenchloride; 10% palladium on activated charcoal; ammonium formate; sodium hydrogencarbonate; lithium tri-t-butoxyaluminum hydride;
In
methanol; diethyl ether; ethanol; water; 1,2-dichloro-ethane; isopropyl alcohol;
DOI:10.1111/j.1747-0285.2010.00995.x
