C₃₅H₃₄Cl₂N₂O₄

Base Information

Chemical Name:C₃₅H₃₄Cl₂N₂O₄
CAS No.:1271212-15-7
Molecular Formula:C₃₅H₃₄Cl₂N₂O₄
Molecular Weight:617.572
Hs Code.:

C<sub>35</sub>H<sub>34</sub>Cl<sub>2</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:

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Chemical Property of C₃₅H₃₄Cl₂N₂O₄

Chemical Property:

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Technology Process of C₃₅H₃₄Cl₂N₂O₄

There total 10 articles about C₃₅H₃₄Cl₂N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 325780-77-6
4,9-bis(ethyloxy)naphtho[2,3-c]furan-1,3-dione

: 1271212-15-7
C₃₅H₃₄Cl₂N₂O₄

Guidance literature:: Multi-step reaction with 9 steps

1: acetic acid / Reflux

2: sodium tetrahydroborate / tetrahydrofuran; methanol

3: triethylsilane; trifluoroacetic acid / dichloromethane

4: water; lithium hydroxide / tetrahydrofuran; methanol

5: dimethylsulfide borane complex / tetrahydrofuran

6: triethylamine / dichloromethane

7: N,N-dimethyl-formamide

8: titanium(IV) isopropylate / tetrahydrofuran

9: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

With titanium(IV) isopropylate; triethylsilane; dmap; sodium tetrahydroborate; dimethylsulfide borane complex; water; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; 8: Kulinkovich reaction / 8: Kulinkovich reaction;
DOI:10.1016/j.bmcl.2010.12.014

Reference yield:

: 1064195-69-2
methyl 4-(4,9-diethoxy-1,3-dioxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzoate

: 1271212-15-7
C₃₅H₃₄Cl₂N₂O₄

Guidance literature:: Multi-step reaction with 8 steps

1: sodium tetrahydroborate / tetrahydrofuran; methanol

2: triethylsilane; trifluoroacetic acid / dichloromethane

3: water; lithium hydroxide / tetrahydrofuran; methanol

4: dimethylsulfide borane complex / tetrahydrofuran

5: triethylamine / dichloromethane

6: N,N-dimethyl-formamide

7: titanium(IV) isopropylate / tetrahydrofuran

8: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

With titanium(IV) isopropylate; triethylsilane; dmap; sodium tetrahydroborate; dimethylsulfide borane complex; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; 7: Kulinkovich reaction / 7: Kulinkovich reaction;
DOI:10.1016/j.bmcl.2010.12.014

Reference yield:

: 1064195-70-5
methyl 4-(4,9-diethoxy-1-hydroxy-3-oxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzoate

: 1271212-15-7
C₃₅H₃₄Cl₂N₂O₄

Guidance literature:: Multi-step reaction with 7 steps

1: triethylsilane; trifluoroacetic acid / dichloromethane

2: water; lithium hydroxide / tetrahydrofuran; methanol

3: dimethylsulfide borane complex / tetrahydrofuran

4: triethylamine / dichloromethane

5: N,N-dimethyl-formamide

6: titanium(IV) isopropylate / tetrahydrofuran

7: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

With titanium(IV) isopropylate; triethylsilane; dmap; dimethylsulfide borane complex; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; 6: Kulinkovich reaction / 6: Kulinkovich reaction;
DOI:10.1016/j.bmcl.2010.12.014