2-(3,5-dihydroxyphenyl)propionate

Base Information

Chemical Name:2-(3,5-dihydroxyphenyl)propionate
CAS No.:101479-00-9
Molecular Formula:C₁₀H₁₂O₄
Molecular Weight:196.203
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(3,5-dihydroxyphenyl)propionate

Chemical Property:

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Technology Process of 2-(3,5-dihydroxyphenyl)propionate

There total 4 articles about 2-(3,5-dihydroxyphenyl)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28924-21-2
3,5-dibenzyloxyacetophenone

: 101479-00-9
2-(3,5-dihydroxyphenyl)propionate

Guidance literature:: Multi-step reaction with 4 steps

1: 63 percent / potassium tert-butoxide / 1,2-dimethoxy-ethane; 2-methyl-propan-2-ol / 2.5 h / Ambient temperature

2: 87 percent / sodium hydroxide (10 percent) / ethanol / 6 h / Heating

3: H₂ / palladium on carbon (10 percent) / ethanol / 2.5 h / 40 °C / 2068.6 Torr

4: H₂SO₄ (conc.) / 12 h / Heating

With sodium hydroxide; sulfuric acid; potassium tert-butylate; hydrogen; palladium on activated charcoal; In 1,2-dimethoxyethane; ethanol; tert-butyl alcohol;
DOI:10.1002/jhet.5570220315

Reference yield:

: 101479-10-1
2-(3',5'-dibenzyloxyphenyl)propionitrile

: 101479-00-9
2-(3,5-dihydroxyphenyl)propionate

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / sodium hydroxide (10 percent) / ethanol / 6 h / Heating

2: H₂ / palladium on carbon (10 percent) / ethanol / 2.5 h / 40 °C / 2068.6 Torr

3: H₂SO₄ (conc.) / 12 h / Heating

With sodium hydroxide; sulfuric acid; hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1002/jhet.5570220315

Reference yield:

: 101479-11-2
2-(3',5'-dibenzyloxyphenyl)propionic acid

: 101479-00-9
2-(3,5-dihydroxyphenyl)propionate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / palladium on carbon (10 percent) / ethanol / 2.5 h / 40 °C / 2068.6 Torr

2: H₂SO₄ (conc.) / 12 h / Heating

With sulfuric acid; hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1002/jhet.5570220315