C₆H₂-1,4-(B(CHCHtBu)2)2-2,5-(Hex)2

Base Information

Chemical Name:C₆H₂-1,4-(B(CHCHtBu)2)2-2,5-(Hex)2
CAS No.:1286246-35-2
Molecular Formula:C₄₂H₇₂B₂
Molecular Weight:598.656
Hs Code.:

C<sub>6</sub>H<sub>2</sub>-1,4-(B(CHCHtBu)2)2-2,5-(Hex)2

Synonyms:

Suppliers and Price of C₆H₂-1,4-(B(CHCHtBu)2)2-2,5-(Hex)2

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆H₂-1,4-(B(CHCHtBu)2)2-2,5-(Hex)2

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆H₂-1,4-(B(CHCHtBu)2)2-2,5-(Hex)2

There total 3 articles about C₆H₂-1,4-(B(CHCHtBu)2)2-2,5-(Hex)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 917-92-0
3,3-Dimethylbut-1-yne

: 1286246-33-0
C₆H₂-1,4-(BH₂(NMe₂Et)2-2,5-(Hex)2

: 1286246-35-2
C₆H₂-1,4-(B(CHCHtBu)2)2-2,5-(Hex)2

Guidance literature:: In benzene; under N2; addn. of benzene to mixt. of boron compd and tert-butylacetylene, vessel frozen at -196°C and evacuated, heating at 60°Cfor 18 h; cooling to room temp., vessel flushed with N2, evapn., purification of oily residue failed;
DOI:10.1039/c0dt01271h

Reference yield:

: 374934-77-7
1,4-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolanyl)-2,5-di-n-hexylbenzene

: 1286246-35-2
C₆H₂-1,4-(B(CHCHtBu)2)2-2,5-(Hex)2

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / diethyl ether / 2.17 h / 0 - 20 °C

1.2: Inert atmosphere

2.1: chloro-trimethyl-silane / tetrahydrofuran / -196 - 20 °C / Inert atmosphere

3.1: benzene / 18 h / 60 °C / sealed vessel; Inert atmosphere

With lithium aluminium tetrahydride; chloro-trimethyl-silane; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1039/c0dt01271h

Reference yield:

: 117635-21-9
1,4-dibromo-2,5-di-n-hexylbenzene

: 1286246-35-2
C₆H₂-1,4-(B(CHCHtBu)2)2-2,5-(Hex)2

Guidance literature:: Multi-step reaction with 4 steps

1.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; methyldi-t-butylphosphine; triethylamine / toluene / 96 h / 90 °C / 250 Torr / sealed vessel; Inert atmosphere

2.1: lithium aluminium tetrahydride / diethyl ether / 2.17 h / 0 - 20 °C

2.2: Inert atmosphere

3.1: chloro-trimethyl-silane / tetrahydrofuran / -196 - 20 °C / Inert atmosphere

4.1: benzene / 18 h / 60 °C / sealed vessel; Inert atmosphere

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; lithium aluminium tetrahydride; chloro-trimethyl-silane; methyldi-t-butylphosphine; triethylamine; In tetrahydrofuran; diethyl ether; toluene; benzene;
DOI:10.1039/c0dt01271h