C₃₂H₃₁BrO₆

Base Information

Chemical Name:C₃₂H₃₁BrO₆
CAS No.:1415228-95-3
Molecular Formula:C₃₂H₃₁BrO₆
Molecular Weight:591.499
Hs Code.:

C<sub>32</sub>H<sub>31</sub>BrO<sub>6</sub>

Synonyms:

Suppliers and Price of C₃₂H₃₁BrO₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₂H₃₁BrO₆

Chemical Property:

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Technology Process of C₃₂H₃₁BrO₆

There total 5 articles about C₃₂H₃₁BrO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1415228-88-4
C₃₅H₃₆O₉

: 1415228-95-3
C₃₂H₃₁BrO₆

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / diethyl ether / 3 h / 0 °C

2: water / 4 h / 20 °C / Acidic conditions

3: carbon tetrabromide; triphenylphosphine / benzene / 17 h / Reflux

With lithium aluminium tetrahydride; carbon tetrabromide; triphenylphosphine; In diethyl ether; water; benzene;
DOI:10.1016/j.bmcl.2012.10.052

Reference yield:

: 1415228-93-1
C₃₂H₃₂O₇

: 1415228-95-3
C₃₂H₃₁BrO₆

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In benzene; for 17h; Reflux;
DOI:10.1016/j.bmcl.2012.10.052

Reference yield:

: 477980-84-0
C₁₀H₁₁FO₃

: 1415228-95-3
C₃₂H₃₁BrO₆

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 120 °C

2: potassium carbonate; 18-crown-6 ether / dichloromethane / 15 h / Reflux

3: palladium 10% on activated carbon; hydrogen; triethylamine / ethyl acetate / 5 h / 20 °C

4: lithium aluminium tetrahydride / diethyl ether / 3 h / 0 °C

5: water / 4 h / 20 °C / Acidic conditions

6: carbon tetrabromide; triphenylphosphine / benzene / 17 h / Reflux

With lithium aluminium tetrahydride; 18-crown-6 ether; carbon tetrabromide; palladium 10% on activated carbon; hydrogen; potassium carbonate; triethylamine; triphenylphosphine; In diethyl ether; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; benzene; 2: |Wittig Olefination;
DOI:10.1016/j.bmcl.2012.10.052