C₁₈H₃₀O₄

Base Information

Chemical Name:C₁₈H₃₀O₄
CAS No.:1609268-89-4
Molecular Formula:C₁₈H₃₀O₄
Molecular Weight:310.434
Hs Code.:

C<sub>18</sub>H<sub>30</sub>O<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₃₀O₄

Chemical Property:

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Technology Process of C₁₈H₃₀O₄

There total 10 articles about C₁₈H₃₀O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1609268-88-3
C₂₈H₃₇NO₆

: 1609268-89-4
C₁₈H₃₀O₄

Guidance literature:: With lithium borohydride; In diethyl ether; water; at 0 - 20 ℃; for 1h; stereoselective reaction; Inert atmosphere;
DOI:10.3987/COM-13-12905

Reference yield:

: C₁₇H₂₆O₅

: 1609268-89-4
C₁₈H₃₀O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; pivaloyl chloride / tetrahydrofuran / 2 h / -20 °C / Inert atmosphere

1.2: 4 h / -20 - 20 °C / Inert atmosphere

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: 3.5 h / Inert atmosphere

3.1: lithium borohydride / diethyl ether; water / 1 h / 0 - 20 °C / Inert atmosphere

With lithium borohydride; sodium hexamethyldisilazane; pivaloyl chloride; triethylamine; In tetrahydrofuran; diethyl ether; water;
DOI:10.3987/COM-13-12905

Reference yield:

: 19790-60-4
3-Benzyloxypropanal

: 1609268-89-4
C₁₈H₃₀O₄

Guidance literature:: Multi-step reaction with 10 steps

1.1: di-n-butylboryl trifluoromethanesulfonate; triethylamine / dichloromethane / -78 °C / Inert atmosphere

1.2: -78 - 0 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine; dmap / dichloromethane / 34 h / Inert atmosphere

3.1: lithium borohydride / diethyl ether; water / 1.16 h / 0 - 20 °C / Inert atmosphere

4.1: [bis(acetoxy)iodo]benzene; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 4.5 h / 20 °C / Inert atmosphere

5.1: benzene / 6.5 h / 80 °C / Inert atmosphere

6.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

7.1: lithium hydroxide hydrate / water; tetrahydrofuran / 2 h / 50 °C / Inert atmosphere

8.1: triethylamine; pivaloyl chloride / tetrahydrofuran / 2 h / -20 °C / Inert atmosphere

8.2: 4 h / -20 - 20 °C / Inert atmosphere

9.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

9.2: 3.5 h / Inert atmosphere

10.1: lithium borohydride / diethyl ether; water / 1 h / 0 - 20 °C / Inert atmosphere

With dmap; lithium borohydride; lithium hydroxide hydrate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; di-n-butylboryl trifluoromethanesulfonate; palladium 10% on activated carbon; hydrogen; sodium hexamethyldisilazane; pivaloyl chloride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane; water; benzene; 1.1: |Evans Aldol Reaction / 5.1: |Wittig Olefination;
DOI:10.3987/COM-13-12905