zirconium⁽⁴⁺⁾ tetraperfluorophenyl-2,6-pyridinedimethoxide dichloride

Base Information

Chemical Name:zirconium⁽⁴⁺⁾ tetraperfluorophenyl-2,6-pyridinedimethoxide dichloride
CAS No.:1312678-50-4
Molecular Formula:C₃₁H₃Cl₂F₂₀NO₂Zr
Molecular Weight:963.468
Hs Code.:

zirconium<sup>(4+)</sup> tetraperfluorophenyl-2,6-pyridinedimethoxide dichloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of zirconium⁽⁴⁺⁾ tetraperfluorophenyl-2,6-pyridinedimethoxide dichloride

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Technology Process of zirconium⁽⁴⁺⁾ tetraperfluorophenyl-2,6-pyridinedimethoxide dichloride

There total 1 articles about zirconium⁽⁴⁺⁾ tetraperfluorophenyl-2,6-pyridinedimethoxide dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1312678-47-9
2,6-bis(di-(pentafluorophenyl)hydroxymethyl)pyridine

: 10026-11-6
zirconium(IV) chloride

: 1312678-50-4
zirconium⁽⁴⁺⁾ tetraperfluorophenyl-2,6-pyridinedimethoxide dichloride

Guidance literature:: With butyllithium; In hexane; toluene; under Ar atm.; to stirred soln. of ligand in toluene under Ar atm. was added soln. of BuLi in hexane at -78°C; mixt. was slowly brought to room temp.; stirred for 4 h; cooled to -78°C; metal salt (1 equiv.) added; mixt. stirred for 12 h; filtered; org. layer evapd.; recrystd. (toluene); elem. anal.;
DOI:10.1134/S0036023611040255