Phenethyltriethoxysilane

Base Information

• Chemical Name: Phenethyltriethoxysilane
• CAS No.: 13340-46-0
• Molecular Formula: C14H24O3Si
• Molecular Weight: 268.428
• European Community (EC) Number: 603-741-3
• DSSTox Substance ID: DTXSID60455153
• Nikkaji Number: J1.196.018I
• Wikidata: Q82277042
• Mol file: 13340-46-0.mol

Synonyms:phenethyltriethoxysilane;phenylethyltriethoxysilane;triethoxy(phenethyl)silane;13340-46-0;phenethyl triethoxysilane;SCHEMBL107467;2-(triethoxysilyl)ethylbenzene;DTXSID60455153;VBSUMMHIJNZMRM-UHFFFAOYSA-N;MFCD11554901

Chemical Property of Phenethyltriethoxysilane

Chemical Property:

• Vapor Pressure: 0.003mmHg at 25°C
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 9
• Exact Mass: 268.14947116
• Heavy Atom Count: 18
• Complexity: 188

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CCO[Si](CCC1=CC=CC=C1)(OCC)OCC

Technology Process of Phenethyltriethoxysilane

There total 21 articles about Phenethyltriethoxysilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + Triethoxysilane (998-30-1) → (2-phenylethyl)triethoxysilane (13340-46-0) + α-phenethyltriethoxysilane (129972-64-1,52886-42-7)

Guidance literature:

methyltriacetoxysilane; platinum; In toluene;

Reference yield: 84.7%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + Triethoxysilane (998-30-1) → (2-methylbenzyl)triethoxysilane + (2-phenylethyl)triethoxysilane (13340-46-0)

Guidance literature:

acetic acid; platinum; In toluene;

Reference yield: 81.0%

Triethoxysilane (998-30-1) + diphenyl acetylene (501-65-5) → triethoxy-[(E)-(1,2-diphenylvinyl)]silane (65119-10-0) + (2-phenylethyl)triethoxysilane (13340-46-0)

Guidance literature:

With chloroplatinic acid 1,1,3,3-tetramethyl-1,3-divinyldisiloxane complex; for 1h; Heating;

DOI:10.1016/0022-328X(92)83082-S

upstream raw materials:

phenethylmagnesium bromide

tetraethoxy orthosilicate

styrene

ethanol

Downstream raw materials:

(2-phenylethyl)triphenylsilane

Refernces

• 1、 Cason,Brooks. "-". . . Retrieved 1954.
• 2、 -. "COMPOUND, AND MANUFACTURING METHOD OF COMPOUND". Paragraph 0044-0045. . Retrieved 2021/06/21.
• 3、 Huo, Yingpeng,Hu, Jiwen,Tu, Yuanyuan,Huang, Zhenzhu,Lin, Shudong,Hu, Yangfei,Feng, Chao. "Platinum-Imidazolyl Schiff Base Complexes Immobilized in Periodic Mesoporous Organosilica Frameworks as Catalysts for Hydrosilylation". . . Retrieved 2020/05/18.