Technology Process of C22H31NO
There total 4 articles about C22H31NO which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium thioethylate;
In
N,N-dimethyl-formamide;
at 130 ℃;
for 20h;
Inert atmosphere;
DOI:10.1021/jm301258w
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine; sodium cyanoborohydride / methanol / 27 h / 20 °C / Inert atmosphere
2: potassium carbonate / N,N-dimethyl-formamide / 73.5 h / 20 - 45 °C / Inert atmosphere
3: sodium thioethylate / N,N-dimethyl-formamide / 20 h / 130 °C / Inert atmosphere
With
sodium cyanoborohydride; potassium carbonate; triethylamine; sodium thioethylate;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm301258w
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine; sodium cyanoborohydride / methanol / 27 h / 20 °C / Inert atmosphere
2: potassium carbonate / N,N-dimethyl-formamide / 73.5 h / 20 - 45 °C / Inert atmosphere
3: sodium thioethylate / N,N-dimethyl-formamide / 20 h / 130 °C / Inert atmosphere
With
sodium cyanoborohydride; potassium carbonate; triethylamine; sodium thioethylate;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm301258w