Technology Process of C32H36N4O3
There total 7 articles about C32H36N4O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: bromine / acetic acid
2: potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran; water / 80 °C
3: sodium hydroxide / tetrahydrofuran; water
4: triethylamine / dichloromethane
5: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; acetone
6: sodium tris(acetoxy)borohydride / dichloromethane
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; osmium(VIII) oxide; bromine; sodium tris(acetoxy)borohydride; potassium carbonate; 4-methylmorpholine N-oxide; triethylamine; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; acetic acid; acetone;
2: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2014.01.012
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran; water / 80 °C
2: sodium hydroxide / tetrahydrofuran; water
3: triethylamine / dichloromethane
4: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; acetone
5: sodium tris(acetoxy)borohydride / dichloromethane
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; osmium(VIII) oxide; sodium tris(acetoxy)borohydride; potassium carbonate; 4-methylmorpholine N-oxide; triethylamine; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; acetone;
1: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2014.01.012
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / dichloromethane
2: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; acetone
3: sodium tris(acetoxy)borohydride / dichloromethane
With
osmium(VIII) oxide; sodium tris(acetoxy)borohydride; 4-methylmorpholine N-oxide; triethylamine;
In
tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1016/j.bmcl.2014.01.012