N-(ethoxycarbonylmethyl)-2-phenyl-4-methyl-5-oxazolecarboxamide

Base Information

Chemical Name:N-(ethoxycarbonylmethyl)-2-phenyl-4-methyl-5-oxazolecarboxamide
CAS No.:1384111-22-1
Molecular Formula:C₁₅H₁₆N₂O₄
Molecular Weight:288.303
Hs Code.:

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Chemical Property of N-(ethoxycarbonylmethyl)-2-phenyl-4-methyl-5-oxazolecarboxamide

Chemical Property:

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Technology Process of N-(ethoxycarbonylmethyl)-2-phenyl-4-methyl-5-oxazolecarboxamide

There total 4 articles about N-(ethoxycarbonylmethyl)-2-phenyl-4-methyl-5-oxazolecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 91137-55-2
4-methyl-2-phenyl-1,3-oxazole-5-carboxylic acid

: 623-33-6
glycine ethyl ester hydrochloride

: 1384111-22-1
N-(ethoxycarbonylmethyl)-2-phenyl-4-methyl-5-oxazolecarboxamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; Inert atmosphere;
DOI:10.3987/COM-13-12865

Reference yield:

: 1556560-87-2
C₅H₄BrNO₂

: 1384111-22-1
N-(ethoxycarbonylmethyl)-2-phenyl-4-methyl-5-oxazolecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / Inert atmosphere

2: selenium(IV) oxide / tetrahydrofuran / Reflux; Inert atmosphere

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / Inert atmosphere

With selenium(IV) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.3987/COM-13-12865

Reference yield:

: 953408-85-0
C₁₁H₉NO₂

: 1384111-22-1
N-(ethoxycarbonylmethyl)-2-phenyl-4-methyl-5-oxazolecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: selenium(IV) oxide / tetrahydrofuran / Reflux; Inert atmosphere

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / Inert atmosphere

With selenium(IV) oxide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.3987/COM-13-12865