Technology Process of C35H41NO3Si
There total 5 articles about C35H41NO3Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C33H35NO4Si; ethylmagnesium bromide;
In
tetrahydrofuran; diethyl ether;
at 0 ℃;
for 1h;
Inert atmosphere;
With
dimethylsulfide borane complex;
In
tetrahydrofuran; diethyl ether;
for 3h;
Inert atmosphere;
Reflux;
DOI:10.1039/c4cc04555f
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine; formaldehyd / dichloromethane / 4 h / 20 °C
1.2: 3 h / 20 °C
2.1: 1H-imidazole / N,N-dimethyl-formamide / 20 h / 20 °C / Inert atmosphere
3.1: tetrahydrofuran; diethyl ether / 1 h / 0 °C / Inert atmosphere
3.2: 3 h / Inert atmosphere; Reflux
With
1H-imidazole; formaldehyd; triethylamine;
In
tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c4cc04555f
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium tetrahydroborate / ethanol / 0 - 20 °C
2.1: dmap / dichloromethane / 0.5 h / 0 °C
3.1: triethylamine; formaldehyd / dichloromethane / 4 h / 20 °C
3.2: 3 h / 20 °C
4.1: 1H-imidazole / N,N-dimethyl-formamide / 20 h / 20 °C / Inert atmosphere
5.1: tetrahydrofuran; diethyl ether / 1 h / 0 °C / Inert atmosphere
5.2: 3 h / Inert atmosphere; Reflux
With
1H-imidazole; dmap; sodium tetrahydroborate; formaldehyd; triethylamine;
In
tetrahydrofuran; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c4cc04555f
