4-(Benzyloxy)-5-methoxy-1H-pyrrolo<2,3-f>chinolin-2,7,9-tricarbonsaeure-trimethylester

Base Information

Chemical Name:4-(Benzyloxy)-5-methoxy-1H-pyrrolo<2,3-f>chinolin-2,7,9-tricarbonsaeure-trimethylester
CAS No.:149049-67-2
Molecular Formula:C₂₅H₂₂N₂O₈
Molecular Weight:478.458
Hs Code.:

Synonyms:

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Chemical Property of 4-(Benzyloxy)-5-methoxy-1H-pyrrolo<2,3-f>chinolin-2,7,9-tricarbonsaeure-trimethylester

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Technology Process of 4-(Benzyloxy)-5-methoxy-1H-pyrrolo<2,3-f>chinolin-2,7,9-tricarbonsaeure-trimethylester

There total 4 articles about 4-(Benzyloxy)-5-methoxy-1H-pyrrolo<2,3-f>chinolin-2,7,9-tricarbonsaeure-trimethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 149049-67-2
4-(Benzyloxy)-5-methoxy-1H-pyrrolo<2,3-f>chinolin-2,7,9-tricarbonsaeure-trimethylester

Guidance literature:: Multi-step reaction with 4 steps

1: 1) KOH / 2) KI / 1) MeOH, r.t., 5 h, 2) r.t., 2 d

2: 91 percent / hydrogen / Raney-nickel / tetrahydrofuran / 32 h / 760 Torr / Ambient temperature

3: 96 percent / 3N HCl / methanol / 4 h / Heating

4: 1) Et₃N, 2) air, HCl(g) / 2) Cu(OAc)2 / 1) CH₂Cl₂, 30 min, 2) CH₂Cl₂, 4 h

With hydrogenchloride; potassium hydroxide; air; hydrogen; triethylamine; copper diacetate; nickel; potassium iodide; In tetrahydrofuran; methanol;
DOI:10.1002/hlca.19930760221

Reference yield:

: 54031-69-5
3-Acetylamino-5,7-dinitro-8-methoxycumarin

: 149049-67-2
4-(Benzyloxy)-5-methoxy-1H-pyrrolo<2,3-f>chinolin-2,7,9-tricarbonsaeure-trimethylester

Guidance literature:: Multi-step reaction with 4 steps

1: 1) KOH / 2) KI / 1) MeOH, r.t., 5 h, 2) r.t., 2 d

2: 91 percent / hydrogen / Raney-nickel / tetrahydrofuran / 32 h / 760 Torr / Ambient temperature

3: 96 percent / 3N HCl / methanol / 4 h / Heating

4: 1) Et₃N, 2) air, HCl(g) / 2) Cu(OAc)2 / 1) CH₂Cl₂, 30 min, 2) CH₂Cl₂, 4 h

With hydrogenchloride; potassium hydroxide; air; hydrogen; triethylamine; copper diacetate; nickel; potassium iodide; In tetrahydrofuran; methanol;
DOI:10.1002/hlca.19930760221

Reference yield:

: α-(Acetylamino)-4',6'-diamino-2'-(benzyloxy)-3'-methoxyzimtsaeure-methylester

: 149049-67-2
4-(Benzyloxy)-5-methoxy-1H-pyrrolo<2,3-f>chinolin-2,7,9-tricarbonsaeure-trimethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / 3N HCl / methanol / 4 h / Heating

2: 1) Et₃N, 2) air, HCl(g) / 2) Cu(OAc)2 / 1) CH₂Cl₂, 30 min, 2) CH₂Cl₂, 4 h

With hydrogenchloride; air; triethylamine; copper diacetate; In methanol;
DOI:10.1002/hlca.19930760221