C₈H₁₂Rh(P(C₆H₅)2CH₂CHCH₂C(CH₂C₆H₅)2CH₂NC(O)C(CH₃)3)⁽¹⁺⁾*SbF₆^(1-)=C₈H₁₂Rh(P(C₆H₅)2CH₂CHCH₂C(CH₂C₆H₅)2CH₂NC(O)C(CH₃)3)SbF₆

Base Information

• Chemical Name: C₈H₁₂Rh(P(C₆H₅)2CH₂CHCH₂C(CH₂C₆H₅)2CH₂NC(O)C(CH₃)3)⁽¹⁺⁾*SbF₆^(1-)=C₈H₁₂Rh(P(C₆H₅)2CH₂CHCH₂C(CH₂C₆H₅)2CH₂NC(O)C(CH₃)3)SbF₆
• CAS No.: 457622-82-1
• Molecular Formula: C₄₄H₅₂NOPRh*F₆Sb
• Molecular Weight: 980.523
• Mol file: 457622-82-1.mol

Synonyms:

Chemical Property of C₈H₁₂Rh(P(C₆H₅)2CH₂CHCH₂C(CH₂C₆H₅)2CH₂NC(O)C(CH₃)3)⁽¹⁺⁾*SbF₆^(1-)=C₈H₁₂Rh(P(C₆H₅)2CH₂CHCH₂C(CH₂C₆H₅)2CH₂NC(O)C(CH₃)3)SbF₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₈H₁₂Rh(P(C₆H₅)2CH₂CHCH₂C(CH₂C₆H₅)2CH₂NC(O)C(CH₃)3)⁽¹⁺⁾*SbF₆^(1-)=C₈H₁₂Rh(P(C₆H₅)2CH₂CHCH₂C(CH₂C₆H₅)2CH₂NC(O)C(CH₃)3)SbF₆

There total 1 articles about C₈H₁₂Rh(P(C₆H₅)2CH₂CHCH₂C(CH₂C₆H₅)2CH₂NC(O)C(CH₃)3)⁽¹⁺⁾*SbF₆^(1-)=C₈H₁₂Rh(P(C₆H₅)2CH₂CHCH₂C(CH₂C₆H₅)2CH₂NC(O)C(CH₃)3)SbF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

silver hexafluoroantimonate (26042-64-8) + chloro(1,5-cyclooctadiene)rhodium(I) dimer + (S)-(-)-1-[4,4-bisbenzyl-2-((diphenylphosphino)methyl)pyrrolidinyl]-2,2-dimethylpropan-1-one (212890-82-9) → C8H12Rh(P(C6H5)2CH2CHCH2C(CH2C6H5)2CH2NC(O)C(CH3)3)(1+)*SbF6(1-)=C8H12Rh(P(C6H5)2CH2CHCH2C(CH2C6H5)2CH2NC(O)C(CH3)3)SbF6 (457622-82-1)

Guidance literature:

In dichloromethane; Sonication; Ar; addn. of CH2Cl2 to a tube contg. Rh complex, Ag salt and ligand, ultrasonication at room temp. for 5 min; centrifugal sedimentation, detected by IR;

DOI:10.1021/ja0261933

upstream raw materials:

silver hexafluoroantimonate

(S)-(-)-1-[4,4-bisbenzyl-2-((diphenylphosphino)methyl)pyrrolidinyl]-2,2-dimethylpropan-1-one