Technology Process of Quinoline, 4-[(1E)-2-phenylethenyl]-
There total 9 articles about Quinoline, 4-[(1E)-2-phenylethenyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1,10-phenanthroline-5,6-dione; trifluorormethanesulfonic acid; oxygen;
In
chlorobenzene;
at 80 ℃;
for 24h;
under 760.051 Torr;
DOI:10.1021/acs.orglett.0c04060
- Guidance literature:
-
With
[Pd2(1,2-bis(diphenylphosphino)ethane)2(SC6H4S)]2(OTf)4; tetrabutylammomium bromide; sodium acetate;
In
N,N-dimethyl acetamide; water;
at 120 ℃;
for 16h;
Inert atmosphere;
DOI:10.1016/j.tetlet.2016.11.085
- Guidance literature:
-
N-Benzylaniline;
With
2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 0.0833333h;
Inert atmosphere;
C6H4NCH2CHCCH2;
In
N,N-dimethyl-formamide;
at 70 ℃;
for 24h;
diastereoselective reaction;
Inert atmosphere;
DOI:10.1002/ejoc.201300368