(-)-6-ethoxy-1-((S)-1-phenylethyl)-2-piperidinone

Base Information

Chemical Name:(-)-6-ethoxy-1-((S)-1-phenylethyl)-2-piperidinone
CAS No.:132363-91-8
Molecular Formula:C₁₅H₂₁NO₂
Molecular Weight:247.337
Hs Code.:

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Chemical Property of (-)-6-ethoxy-1-((S)-1-phenylethyl)-2-piperidinone

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Technology Process of (-)-6-ethoxy-1-((S)-1-phenylethyl)-2-piperidinone

There total 5 articles about (-)-6-ethoxy-1-((S)-1-phenylethyl)-2-piperidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

: 126017-74-1
(S)-1-(1-phenylethyl)piperidine-2,6-dione

: 132363-93-0
(-)-3,4-dihydro-1-((S)-1-phenylethyl)-2-pyridinone

: 132363-91-8,132363-92-9
(-)-6-ethoxy-1-((S)-1-phenylethyl)-2-piperidinone

Guidance literature:: With hydrogenchloride; sodium tetrahydroborate; at 0 - 5 ℃; for 3h; Yields of byproduct given;

Reference yield: 5.0%

: 64-17-5
ethanol

: 126017-74-1
(S)-1-(1-phenylethyl)piperidine-2,6-dione

: 132363-93-0
(-)-3,4-dihydro-1-((S)-1-phenylethyl)-2-pyridinone

: 132363-91-8,132363-92-9
(-)-6-ethoxy-1-((S)-1-phenylethyl)-2-piperidinone

Guidance literature:: With hydrogenchloride; sodium tetrahydroborate; at 0 - 5 ℃; for 3h; Yield given;

Reference yield:

: 108-55-4
glutaric anhydride,

: 132363-91-8,132363-92-9
(-)-6-ethoxy-1-((S)-1-phenylethyl)-2-piperidinone

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 6 h / Heating

2: acetyl chloride / toluene / 5 h / Heating

3: sodium borohydride, 2N HCl / 3 h / 0 - 5 °C

With hydrogenchloride; sodium tetrahydroborate; acetyl chloride; In toluene;