Technology Process of (E) 3-phenylthiopent-3-en-2-one
There total 4 articles about (E) 3-phenylthiopent-3-en-2-one which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
methanesulfonic acid; acetic anhydride;
In
dichloromethane;
at 40 ℃;
for 2h;
Yield given. Yields of byproduct given;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 65 percent / K-tert-butoxide / tetrahydrofuran / 4.5 h / 0 - 20 °C / Heating
2: 73 percent / meta-chloroperbenzoic acid / diethyl ether / 0.5 h / 0 °C
3: acetic anhydride, methanesulphonic acid / CH2Cl2 / 2 h / 40 °C
With
methanesulfonic acid; potassium tert-butylate; acetic anhydride; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; diethyl ether; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: toluene-p-sulphonic acid / benzene / Heating
2: 73 percent / meta-chloroperbenzoic acid / diethyl ether / 0.5 h / 0 °C
3: acetic anhydride, methanesulphonic acid / CH2Cl2 / 2 h / 40 °C
With
methanesulfonic acid; acetic anhydride; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid;
In
diethyl ether; dichloromethane; benzene;