C₁₈H₁₁BrCl₂FN₅O₂

Base Information

Chemical Name:C₁₈H₁₁BrCl₂FN₅O₂
CAS No.:1093257-24-9
Molecular Formula:C₁₈H₁₁BrCl₂FN₅O₂
Molecular Weight:499.126
Hs Code.:

C<sub>18</sub>H<sub>11</sub>BrCl<sub>2</sub>FN<sub>5</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₁₈H₁₁BrCl₂FN₅O₂

Chemical Property:

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Technology Process of C₁₈H₁₁BrCl₂FN₅O₂

There total 7 articles about C₁₈H₁₁BrCl₂FN₅O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1093265-60-1
2-azido-N-({4-bromo-3-[(3-chloro-5-cyanophenyl)oxy]-2-fluorophenyl}methyl)-4-chloro-1H-imidazole-5-carboxamide

: 1093257-24-9
C₁₈H₁₁BrCl₂FN₅O₂

Guidance literature:: With hydrogen; In ethyl acetate; for 7h; under 2585.81 Torr;
DOI:10.1021/jm301294g

Reference yield:

: C₉H₁₁BBrFO₂

: 1093257-24-9
C₁₈H₁₁BrCl₂FN₅O₂

Guidance literature:: Multi-step reaction with 6 steps

1: dihydrogen peroxide; acetic acid / water / 20 °C

2: potassium carbonate / N,N-dimethyl acetamide / 7 h / 150 °C

3: dibenzoyl peroxide; N-Bromosuccinimide / 1,2-dichloro-ethane / 20 h / Reflux

4: ammonia / dichloromethane; methanol / 10 - 20 °C

5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

6: hydrogen / ethyl acetate / 7 h / 2585.81 Torr

With N-Bromosuccinimide; ammonia; hydrogen; dihydrogen peroxide; potassium carbonate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dibenzoyl peroxide; In methanol; dichloromethane; N,N-dimethyl acetamide; water; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/jm301294g

Reference yield:

: 1093265-24-7
3-(6-bromo-2-fluoro-3-methylphenoxy)-5-chlorobenzonitrile

: 1093257-24-9
C₁₈H₁₁BrCl₂FN₅O₂

Guidance literature:: Multi-step reaction with 4 steps

1: dibenzoyl peroxide; N-Bromosuccinimide / 1,2-dichloro-ethane / 20 h / Reflux

2: ammonia / dichloromethane; methanol / 10 - 20 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

4: hydrogen / ethyl acetate / 7 h / 2585.81 Torr

With N-Bromosuccinimide; ammonia; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dibenzoyl peroxide; In methanol; dichloromethane; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/jm301294g