[(η(5)-C5H5)Fe(η(5)-C5H4C2)]Si(C6H5)2(CH2)3CH3

Base Information

Chemical Name:[(η(5)-C5H5)Fe(η(5)-C5H4C2)]Si(C6H5)2(CH2)3CH3
CAS No.:222552-12-7
Molecular Formula:C₂₈H₂₈FeSi
Molecular Weight:448.463
Hs Code.:

Synonyms:

Suppliers and Price of [(η(5)-C5H5)Fe(η(5)-C5H4C2)]Si(C6H5)2(CH2)3CH3

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [(η(5)-C5H5)Fe(η(5)-C5H4C2)]Si(C6H5)2(CH2)3CH3

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [(η(5)-C5H5)Fe(η(5)-C5H4C2)]Si(C6H5)2(CH2)3CH3

There total 1 articles about [(η(5)-C5H5)Fe(η(5)-C5H4C2)]Si(C6H5)2(CH2)3CH3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 1271-47-2
ferroceneacetylene

: 80-10-4
diphenylsilyl dichloride

: 55997-98-3
[(η(5)-C5H5)Fe(η(5)-C5H4C2)]2Si(C6H5)2

: 222552-12-7
[(η(5)-C5H5)Fe(η(5)-C5H4C2)]Si(C6H5)2(CH2)3CH3

Guidance literature:: With BuLi; In tetrahydrofuran; inert atmosphere; addn. of 1.1 equiv. of BuLi (in hexanes) to Fe-complex soln. (in THF) at -78°C, addn. of 0.5 equiv. of silane (after 30 min), warming to room temp. during 30 min, stirring for 2 h; hydrolyzing (-5°C), extn. into CH2Cl2, washing of org. layer (H2O), drying (over MgSO4), solvent removal, chromy. (SiO2, CH2Cl2/hexane=1:10, then 1:1); elem. anal.;
DOI:10.1016/S0022-328X(98)00597-X

Reference yield:

: dicobalt octacarbonyl

: 222552-12-7
[(η(5)-C5H5)Fe(η(5)-C5H4C2)]Si(C6H5)2(CH2)3CH3

: 222552-54-7
[(η(5)-C5H5)Fe(η(5)-C5H4C(Co2(CO)6)C)]SiPh2Bu

Guidance literature:: In hexane; N2-atmosphere; stirring Fe-complex with 2 equiv. of Co-complex for 30 min; solvent removal; elem. anal.;
DOI:10.1016/S0022-328X(98)00597-X