C₂₃H₂₆N₆O₂S

Base Information

Chemical Name:C₂₃H₂₆N₆O₂S
CAS No.:1351811-41-0
Molecular Formula:C₂₃H₂₆N₆O₂S
Molecular Weight:450.564
Hs Code.:

C<sub>23</sub>H<sub>26</sub>N<sub>6</sub>O<sub>2</sub>S

Synonyms:

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Chemical Property of C₂₃H₂₆N₆O₂S

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Technology Process of C₂₃H₂₆N₆O₂S

There total 10 articles about C₂₃H₂₆N₆O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1351813-11-0
3-(5-(cyclohexylamino)-6-(1-methyl-1H-pyrazol-4-yl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-indazol-3-yl)benzenesulfonamide

: 1351811-41-0
C₂₃H₂₆N₆O₂S

Guidance literature:: With tetrabutyl ammonium fluoride; ethylenediamine; In tetrahydrofuran; for 24h; Reflux;
DOI:10.1021/jm4000215

Reference yield:

: 1351813-04-1
C₁₇H₂₃N₅O₃Si

: 1351811-41-0
C₂₃H₂₆N₆O₂S

Guidance literature:: Multi-step reaction with 6 steps

1.1: tetrabutyl ammonium fluoride; ethylenediamine / tetrahydrofuran / 8 h / Reflux

2.1: iodine; potassium hydroxide / N,N-dimethyl-formamide / 2 h / 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.67 h / 0 - 20 °C

3.2: 3 h / Inert atmosphere; Reflux

4.1: ethanol; iron; ammonium chloride / water / 0.75 h / Reflux

5.1: sodium tris(acetoxy)borohydride; acetic acid / dichloromethane / 3 h / 20 °C

6.1: tetrabutyl ammonium fluoride; ethylenediamine / tetrahydrofuran / 24 h / Reflux

With ethanol; tetrabutyl ammonium fluoride; iodine; sodium tris(acetoxy)borohydride; iron; sodium hydride; ammonium chloride; acetic acid; ethylenediamine; potassium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; 1.1: |Suzuki Coupling / 3.2: |Suzuki Coupling;
DOI:10.1021/jm4000215

Reference yield:

: 1351813-03-0
C₁₃H₁₈BrN₃O₃Si

: 1351811-41-0
C₂₃H₂₆N₆O₂S

Guidance literature:: Multi-step reaction with 7 steps

1.1: dichloro[1,1'-bis(di-t-butylphosphino)ferrocene]palladium(II); potassium carbonate / tetrahydrofuran; water / 3.5 h / Reflux; Inert atmosphere

2.1: tetrabutyl ammonium fluoride; ethylenediamine / tetrahydrofuran / 8 h / Reflux

3.1: iodine; potassium hydroxide / N,N-dimethyl-formamide / 2 h / 20 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 0.67 h / 0 - 20 °C

4.2: 3 h / Inert atmosphere; Reflux

5.1: ethanol; iron; ammonium chloride / water / 0.75 h / Reflux

6.1: sodium tris(acetoxy)borohydride; acetic acid / dichloromethane / 3 h / 20 °C

7.1: tetrabutyl ammonium fluoride; ethylenediamine / tetrahydrofuran / 24 h / Reflux

With dichloro[1,1'-bis(di-t-butylphosphino)ferrocene]palladium(II); ethanol; tetrabutyl ammonium fluoride; iodine; sodium tris(acetoxy)borohydride; iron; sodium hydride; potassium carbonate; ammonium chloride; acetic acid; ethylenediamine; potassium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; 1.1: |Suzuki Coupling / 2.1: |Suzuki Coupling / 4.2: |Suzuki Coupling;
DOI:10.1021/jm4000215