C₃₁H₃₁N₃O₄S₂

Base Information

• Chemical Name: C₃₁H₃₁N₃O₄S₂
• CAS No.: 1394355-98-6
• Molecular Formula: C₃₁H₃₁N₃O₄S₂
• Molecular Weight: 573.737
• Mol file: 1394355-98-6.mol

Synonyms:

Chemical Property of C₃₁H₃₁N₃O₄S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₁H₃₁N₃O₄S₂

There total 4 articles about C₃₁H₃₁N₃O₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(3-piperidin-1-ylpropoxy)phenylamine (251552-34-8) → C31H31N3O4S2 (1394355-98-6)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol; water / Reflux

2: sodium acetate / acetic acid / Reflux

With sodium acetate; In ethanol; water; acetic acid;

DOI:10.1016/j.bmcl.2012.06.088

Reference yield:

1-[3-(4-nitro-phenoxy)-propyl]-piperidine (92374-75-9) → C31H31N3O4S2 (1394355-98-6)

Guidance literature:

Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / methanol

2: ethanol; water / Reflux

3: sodium acetate / acetic acid / Reflux

With palladium 10% on activated carbon; hydrogen; sodium acetate; In methanol; ethanol; water; acetic acid;

DOI:10.1016/j.bmcl.2012.06.088

Reference yield:

1-(4-bromobutoxy)-4-nitrobenzene (55502-03-9) → C31H31N3O4S2 (1394355-98-6)

Guidance literature:

Multi-step reaction with 4 steps

1: potassium carbonate / acetonitrile / 80 °C

2: palladium 10% on activated carbon; hydrogen / methanol

3: ethanol; water / Reflux

4: sodium acetate / acetic acid / Reflux

With palladium 10% on activated carbon; hydrogen; sodium acetate; potassium carbonate; In methanol; ethanol; water; acetic acid; acetonitrile;

DOI:10.1016/j.bmcl.2012.06.088

upstream raw materials:

4-(4-formylphenoxy)benzamide

C₁₇H₂₂N₂O₂S₂

4-(3-piperidin-1-ylpropoxy)phenylamine

1-[3-(4-nitro-phenoxy)-propyl]-piperidine