C₂₅H₃₀N₂O₃S₂

Base Information

Chemical Name:C₂₅H₃₀N₂O₃S₂
CAS No.:1374354-86-5
Molecular Formula:C₂₅H₃₀N₂O₃S₂
Molecular Weight:470.657
Hs Code.:

C<sub>25</sub>H<sub>30</sub>N<sub>2</sub>O<sub>3</sub>S<sub>2</sub>

Synonyms:

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Chemical Property of C₂₅H₃₀N₂O₃S₂

Chemical Property:

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Technology Process of C₂₅H₃₀N₂O₃S₂

There total 17 articles about C₂₅H₃₀N₂O₃S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374354-76-3
C₁₆H₂₉NO₃SSi

: 1374354-86-5
C₂₅H₃₀N₂O₃S₂

Guidance literature:: Multi-step reaction with 10 steps

1: diethyl ether

2: sodium hexamethyldisilazane; triethylamine / tetrahydrofuran

3: N-Bromosuccinimide / tetrahydrofuran

4: sodium diformamide / acetonitrile

5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

6: 1H-imidazole / N,N-dimethyl-formamide

7: Lawessons reagent; pyridine / toluene / 100 °C

8: tetrabutyl ammonium fluoride / tetrahydrofuran

9: thionyl chloride / toluene

10: N-ethyl-N,N-diisopropylamine / acetonitrile

With Lawessons reagent; pyridine; 1H-imidazole; N-Bromosuccinimide; thionyl chloride; sodium diformamide; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067

Reference yield:

: 1374354-78-5
C₉H₁₃NO₂S*ClH

: 1374354-86-5
C₂₅H₃₀N₂O₃S₂

Guidance literature:: Multi-step reaction with 6 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

2: 1H-imidazole / N,N-dimethyl-formamide

3: Lawessons reagent; pyridine / toluene / 100 °C

4: tetrabutyl ammonium fluoride / tetrahydrofuran

5: thionyl chloride / toluene

6: N-ethyl-N,N-diisopropylamine / acetonitrile

With Lawessons reagent; pyridine; 1H-imidazole; thionyl chloride; tetrabutyl ammonium fluoride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067

Reference yield:

: 185147-08-4
4-fluoro-3-methylbenzonitrile

: 1374354-86-5
C₂₅H₃₀N₂O₃S₂

Guidance literature:: Multi-step reaction with 8 steps

1: sodium hydride

2: sodium hydroxide

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

4: 1H-imidazole / N,N-dimethyl-formamide

5: Lawessons reagent; pyridine / toluene / 100 °C

6: tetrabutyl ammonium fluoride / tetrahydrofuran

7: thionyl chloride / toluene

8: N-ethyl-N,N-diisopropylamine / acetonitrile

With Lawessons reagent; pyridine; 1H-imidazole; thionyl chloride; tetrabutyl ammonium fluoride; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067