[(CH(CH₃)2)2C₆H₃NCCH₃]2CHMnIC₄H₈O

Base Information

Chemical Name:[(CH(CH₃)2)2C₆H₃NCCH₃]2CHMnIC₄H₈O
CAS No.:727427-53-4
Molecular Formula:C₃₃H₄₉IMnN₂O
Molecular Weight:671.607
Hs Code.:

[(CH(CH<sub>3</sub>)2)2C<sub>6</sub>H<sub>3</sub>NCCH<sub>3</sub>]2CHMnIC<sub>4</sub>H<sub>8</sub>O

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Chemical Property of [(CH(CH₃)2)2C₆H₃NCCH₃]2CHMnIC₄H₈O

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Technology Process of [(CH(CH₃)2)2C₆H₃NCCH₃]2CHMnIC₄H₈O

There total 1 articles about [(CH(CH₃)2)2C₆H₃NCCH₃]2CHMnIC₄H₈O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 7790-33-2
manganese(II) iodide

: 205993-24-4
HC(CMeN-2,6-i-Pr₂C₆H₃)2K

: 727427-53-4
[(CH(CH₃)2)2C₆H₃NCCH₃]2CHMnIC₄H₈O

Guidance literature:: In tetrahydrofuran; byproducts: KI; ligand in THF added to suspn. of MnI2 in THF at -78°, warmed to room temp., stirred for 14 h; filtered, concd., crystd. at -26°C for 24 h, elem. anal.;
DOI:10.1002/ejic.200300289

Reference yield: 96.0%

: 727427-53-4
[(CH(CH₃)2)2C₆H₃NCCH₃]2CHMnIC₄H₈O

: 676264-72-5
[HC(CMeN(2,6-diisopropylphenyl))2]bis(μ-iodo)dimanganese(II)

Guidance literature:: In toluene; refluxed in toluene for 0.5 h; evapd.(vac.), elem. anal.;
DOI:10.1002/ejic.200300289

Reference yield:

: 727427-53-4
[(CH(CH₃)2)2C₆H₃NCCH₃]2CHMnIC₄H₈O

: [(CH(CH₃)2)2C₆H₃NCCH₃]2CHMnNH(CH(CH₃)2)2C₆H₃C[(CH(CH₃)2NCCH₃)2]

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: K₂Na alloy / toluene

With K₂Na alloy; In tetrahydrofuran; toluene;
DOI:10.1002/ejic.200300289