C₃₃H₂₈ClN₃O

Base Information

Chemical Name:C₃₃H₂₈ClN₃O
CAS No.:1283596-43-9
Molecular Formula:C₃₃H₂₈ClN₃O
Molecular Weight:518.058
Hs Code.:

C<sub>33</sub>H<sub>28</sub>ClN<sub>3</sub>O

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₂₈ClN₃O

Chemical Property:

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Technology Process of C₃₃H₂₈ClN₃O

There total 7 articles about C₃₃H₂₈ClN₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1309877-90-4
C₂₆H₂₄ClIN₂O

: 4-ethynylpyridine hydrochloride

: 1283596-43-9
C₃₃H₂₈ClN₃O

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.01.006

Reference yield:

: 1283596-51-9
C₁₅H₁₂ClN*ClH

: 1283596-43-9
C₃₃H₂₈ClN₃O

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / 1,2-dichloro-ethane / 18 h

1.2: 1 h

2.1: 1,2-dichloro-ethane / 4 h

3.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / N,N-dimethyl-formamide

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; acetic acid; triethylamine; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; 3.1: Sonogashira coupling;
DOI:10.1016/j.bmcl.2011.01.006

Reference yield:

: C₂₂H₁₇ClIN

: 1283596-43-9
C₃₃H₂₈ClN₃O

Guidance literature:: Multi-step reaction with 2 steps

1: 1,2-dichloro-ethane / 4 h

2: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / N,N-dimethyl-formamide

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; 2: Sonogashira coupling;
DOI:10.1016/j.bmcl.2011.01.006