(2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(OMe)2

Base Information

Chemical Name:(2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(OMe)2
CAS No.:1185739-13-2
Molecular Formula:C₄₂H₇₆GeN₄O₂
Molecular Weight:741.681
Hs Code.:

(2,6-[CH<sub>2</sub>N(iPr)2]2C<sub>6</sub>H<sub>3</sub>)2Ge(OMe)2

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Chemical Property of (2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(OMe)2

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Technology Process of (2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(OMe)2

There total 1 articles about (2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(OMe)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 2,6-bis(diisopropylaminomethyl)phenyllithium

: tetramethoxygermanium

: 1185739-13-2
(2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(OMe)2

Guidance literature:: In tetrahydrofuran; under inert atm. ArLi in THF was added dropwise to soln. Ge(OMe)4 in THFat -78°C and stirred at room temp. for 1 h; soln. was filtered through Celite, concd. in vacuo and crystd. in pentane at -20°C; elem. anal.;
DOI:10.1002/ejic.200800494

Reference yield: 78.0%

: 1185739-13-2
(2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(OMe)2

: 7732-18-5
water

: 11113-87-4
silver fluoride

: 1185739-14-3
(2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(F)OH

Guidance literature:: In toluene; under N2 atm. soln. Ge complex, H2O and AgF in toluene in sealed tube were heated at 110°C for 6 h; solvent was removed in vacuo, pentane was added, soln. was filtered, solvent was removed; elem. anal.;
DOI:10.1002/ejic.200800494

Reference yield: 30.0%

: 1185739-13-2
(2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(OMe)2

: 7732-18-5
water

: 1185739-17-6
(2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(OH)2

Guidance literature:: With Bu₄NF; In tetrahydrofuran; toluene; under inert atm. soln. Ge complex and Bu4NF in THF containing H2O in toluene was heated at reflux for 3 h; solvent was removed in vacuo, residue was solubilized in pentane and crystd. at -20°C; elem. anal.;
DOI:10.1002/ejic.200800494