4-methoxy-5-[7-(4-methoxycarbonyl-butyl)-1H-indole-3-carbonyl]-3-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-furan-2-carboxylic acid methyl ester

Base Information

Chemical Name:4-methoxy-5-[7-(4-methoxycarbonyl-butyl)-1H-indole-3-carbonyl]-3-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-furan-2-carboxylic acid methyl ester
CAS No.:1310382-65-0
Molecular Formula:C₃₇H₃₄N₂O₉S
Molecular Weight:682.751
Hs Code.:

4-methoxy-5-[7-(4-methoxycarbonyl-butyl)-1H-indole-3-carbonyl]-3-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-furan-2-carboxylic acid methyl ester

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Chemical Property of 4-methoxy-5-[7-(4-methoxycarbonyl-butyl)-1H-indole-3-carbonyl]-3-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-furan-2-carboxylic acid methyl ester

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Technology Process of 4-methoxy-5-[7-(4-methoxycarbonyl-butyl)-1H-indole-3-carbonyl]-3-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-furan-2-carboxylic acid methyl ester

There total 8 articles about 4-methoxy-5-[7-(4-methoxycarbonyl-butyl)-1H-indole-3-carbonyl]-3-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-furan-2-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 915377-45-6
5-(1H-indol-7-yl)-pentanoic acid methyl ester

: C₂₃H₁₈ClNO₇S

: 1310382-65-0
4-methoxy-5-[7-(4-methoxycarbonyl-butyl)-1H-indole-3-carbonyl]-3-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-furan-2-carboxylic acid methyl ester

Guidance literature:: With diethylaluminium chloride; In hexane; dichloromethane; at 0 - 20 ℃; for 15h;
DOI:10.1002/ddr.20391

Reference yield:

: 890120-49-7
3-methoxy-4[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-furan-2,5-dicarboxylic acid dimethyl ester

: 1310382-65-0
4-methoxy-5-[7-(4-methoxycarbonyl-butyl)-1H-indole-3-carbonyl]-3-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-furan-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: water; lithium hydroxide

2: dmap; oxalyl dichloride / 0.33 h / 20 °C

3: diethylaluminium chloride / hexane; dichloromethane / 15 h / 0 - 20 °C

With dmap; oxalyl dichloride; water; diethylaluminium chloride; lithium hydroxide; In hexane; dichloromethane;
DOI:10.1002/ddr.20391

Reference yield:

: 149108-61-2
1-tosyl-1H-indol-3-boronic acid

: 1310382-65-0
4-methoxy-5-[7-(4-methoxycarbonyl-butyl)-1H-indole-3-carbonyl]-3-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-furan-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / N,N-dimethyl-formamide / 12 h / 90 °C

2: water; lithium hydroxide

3: dmap; oxalyl dichloride / 0.33 h / 20 °C

4: diethylaluminium chloride / hexane; dichloromethane / 15 h / 0 - 20 °C

With dmap; bis-triphenylphosphine-palladium(II) chloride; oxalyl dichloride; water; diethylaluminium chloride; sodium carbonate; lithium hydroxide; In hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ddr.20391