[OsH(κ2-O2CCH3)(CCH=CPh2)(P(i-Pr)3)2]BF4

Base Information

• Chemical Name: [OsH(κ2-O2CCH3)(CCH=CPh2)(P(i-Pr)3)2]BF4
• CAS No.: 936073-49-3
• Molecular Formula: BF₄*C₃₅H₅₇O₂OsP₂
• Molecular Weight: 848.789

Synonyms:

Chemical Property of [OsH(κ2-O2CCH3)(CCH=CPh2)(P(i-Pr)3)2]BF4

Chemical Property:

Purity/Quality:

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Technology Process of [OsH(κ2-O2CCH3)(CCH=CPh2)(P(i-Pr)3)2]BF4

There total 1 articles about [OsH(κ2-O2CCH3)(CCH=CPh2)(P(i-Pr)3)2]BF4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

[OsH(=C=C=CPh2)(CH3CN)2(P(i-Pr)3)2]BF4 + acetic acid (64-19-7,77671-22-8) → [OsH(κ2-O2CCH3)(CCH=CPh2)(P(i-Pr)3)2]BF4 (936073-49-3)

Guidance literature:

In dichloromethane; acetic acid; byproducts: CH3CN; Schlenk technique; soln. of Os complex in CH2Cl2 was treated with acid; mixt. was stirred at room temp. for 30 min; filtered through Celite; evapd.; Et2O added; filtered; washed (Et2O); dried (vac.); elem. anal.;

DOI:10.1021/om0611655

Reference yield:

[D3]acetonitrile (2206-26-0) + [OsH(κ2-O2CCH3)(CCH=CPh2)(P(i-Pr)3)2]BF4 (936073-49-3) → [OsH(κ1-O2CCH3)(CD3CN)(CCH=CPh2)(P(i-Pr)3)2]BF4

Guidance literature:

In [D₃]acetonitrile; Schlenk technique; Os complex was dissolved in CD3CN; NMR monitoring; not isolated;

DOI:10.1021/om0611655

upstream raw materials:

acetic acid

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