Technology Process of C15H10BrNO
There total 3 articles about C15H10BrNO which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol / 2.5 h / Reflux; Inert atmosphere
2: 3-chloro-benzenecarboperoxoic acid / chloroform / 0.17 h / Reflux; Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
ethanol; chloroform;
1: Suzuki coupling;
DOI:10.1021/jm200544q
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogenchloride; sodium nitrite / water / 0.25 h / Cooling with ice; Inert atmosphere
1.2: 0.17 h / Inert atmosphere
2.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol / 2.5 h / Reflux; Inert atmosphere
3.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 0.17 h / Reflux; Inert atmosphere
With
hydrogenchloride; tetrakis(triphenylphosphine) palladium(0); potassium carbonate; 3-chloro-benzenecarboperoxoic acid; sodium nitrite;
In
ethanol; chloroform; water;
2.1: Suzuki coupling;
DOI:10.1021/jm200544q
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
chloroform;
for 0.166667h;
Reflux;
Inert atmosphere;
DOI:10.1021/jm200544q