4-chlorophenylaldazine di-N-oxide

Base Information

Chemical Name:4-chlorophenylaldazine di-N-oxide
CAS No.:23879-15-4
Molecular Formula:C₁₄H₁₀Cl₂N₂O₂
Molecular Weight:309.152
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-chlorophenylaldazine di-N-oxide

Chemical Property:

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Technology Process of 4-chlorophenylaldazine di-N-oxide

There total 3 articles about 4-chlorophenylaldazine di-N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 3848-36-0
4-chlorobenzaldoxime

: 23879-15-4,149019-19-2
4-chlorophenylaldazine di-N-oxide

Guidance literature:: With dihydrogen peroxide; In water; at 20 ℃; for 5h; horseradish peroxidase;
DOI:10.1055/s-1991-26433

Reference yield: 65.0%

: 3717-24-6
4-chlorobenzaldehyde oxime

: 23879-15-4,149019-19-2
4-chlorophenylaldazine di-N-oxide

Guidance literature:: With ammonium cerium(IV) nitrate; In acetone; at 0 ℃; for 0.0833333h;

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 23879-15-4,149019-19-2
4-chlorophenylaldazine di-N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: NH₂OH*HCl, AcONa / methanol / 0.5 h / Heating

2: 65 percent / CAN / acetone / 0.08 h / 0 °C

With ammonium cerium(IV) nitrate; hydroxylamine hydrochloride; sodium acetate; In methanol; acetone;