C₄₉H₅₉NOSi₂

Base Information

Chemical Name:C₄₉H₅₉NOSi₂
CAS No.:1379684-14-6
Molecular Formula:C₄₉H₅₉NOSi₂
Molecular Weight:734.185
Hs Code.:

C<sub>49</sub>H<sub>59</sub>NOSi<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₉H₅₉NOSi₂

Chemical Property:

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Technology Process of C₄₉H₅₉NOSi₂

There total 5 articles about C₄₉H₅₉NOSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1379684-11-3
C₅₄H₆₇NO₂Si₂

: 1379684-14-6
C₄₉H₅₉NOSi₂

Guidance literature:: With toluene-4-sulfonic acid; In methanol; dichloromethane; at 20 ℃;
DOI:10.1039/c2jm30978e

Reference yield:

: 80278-94-0
1,2,3,3a,4,8b-hexahydrocyclopent[b]indole

: 1379684-14-6
C₄₉H₅₉NOSi₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: palladium diacetate; johnphos; sodium t-butanolate / toluene / Reflux

2.1: N-Bromosuccinimide / acetone / 5 h / 20 °C / Inert atmosphere

3.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0.75 h / -78 °C / Inert atmosphere

3.2: 25 °C / Inert atmosphere

4.1: bis(tri-tert-butylphosphine)palladium⁽⁰⁾; caesium carbonate / tetrahydrofuran / Reflux; Inert atmosphere

5.1: toluene-4-sulfonic acid / methanol; dichloromethane / 20 °C

With N-Bromosuccinimide; bis(tri-tert-butylphosphine)palladium⁽⁰⁾; tert.-butyl lithium; palladium diacetate; caesium carbonate; toluene-4-sulfonic acid; johnphos; sodium t-butanolate; In tetrahydrofuran; methanol; dichloromethane; acetone; toluene; pentane;
DOI:10.1039/c2jm30978e

Reference yield:

: 1250863-85-4
7-bromo-1,2,3,3a,4,8b-hexahydro-4-(4-methylphenyl)-cyclopent-[b]indole

: 1379684-14-6
C₄₉H₅₉NOSi₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0.75 h / -78 °C / Inert atmosphere

1.2: 25 °C / Inert atmosphere

2.1: bis(tri-tert-butylphosphine)palladium⁽⁰⁾; caesium carbonate / tetrahydrofuran / Reflux; Inert atmosphere

3.1: toluene-4-sulfonic acid / methanol; dichloromethane / 20 °C

With bis(tri-tert-butylphosphine)palladium⁽⁰⁾; tert.-butyl lithium; caesium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane; pentane;
DOI:10.1039/c2jm30978e