C₂₇H₂₆N₄O₄S₂

Base Information

Chemical Name:C₂₇H₂₆N₄O₄S₂
CAS No.:1613315-69-7
Molecular Formula:C₂₇H₂₆N₄O₄S₂
Molecular Weight:534.66
Hs Code.:

C<sub>27</sub>H<sub>26</sub>N<sub>4</sub>O<sub>4</sub>S<sub>2</sub>

Synonyms:

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Chemical Property of C₂₇H₂₆N₄O₄S₂

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Technology Process of C₂₇H₂₆N₄O₄S₂

There total 8 articles about C₂₇H₂₆N₄O₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1613316-26-9
C₃₀H₃₂N₄O₄S₂

: 1613315-69-7
C₂₇H₂₆N₄O₄S₂

Guidance literature:: With methanol; sodium hydroxide; at 20 ℃; for 18h;
DOI:10.1016/j.bmcl.2014.04.078

Reference yield:

: 180977-38-2
4-nitro-2-(1-naphthyl)benzoic acid methyl ester

: 1613315-69-7
C₂₇H₂₆N₄O₄S₂

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydroxide; methanol / 3 h / 60 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol / dichloromethane / 20 °C

3: tin(ll) chloride / ethyl acetate / 3 h / Reflux

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

5: formic acid / dichloromethane / 20 °C

6: sodium hydroxide; methanol / 18 h / 20 °C

With methanol; formic acid; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; tin(ll) chloride; sodium hydroxide; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.04.078

Reference yield:

: 180977-37-1
4-nitro-2-(1-naphthyl)benzoic acid

: 1613315-69-7
C₂₇H₂₆N₄O₄S₂

Guidance literature:: Multi-step reaction with 5 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol / dichloromethane / 20 °C

2: tin(ll) chloride / ethyl acetate / 3 h / Reflux

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

4: formic acid / dichloromethane / 20 °C

5: sodium hydroxide; methanol / 18 h / 20 °C

With methanol; formic acid; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; tin(ll) chloride; sodium hydroxide; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.04.078