Technology Process of C37H51F2N9O6
There total 10 articles about C37H51F2N9O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N,N-tetramethyluroniumhexafluorophosphate;
In
N,N-dimethyl-formamide;
at 20 ℃;
DOI:10.1016/j.bmcl.2014.10.057
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 20 °C
2: N-ethyl-N,N-diisopropylamine; ammonium acetate / o-xylene / Reflux
3: hydrogenchloride / 1,4-dioxane / 20 °C
4: O-(benzotriazol-1-yl)-N,N,N,N-tetramethyluroniumhexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C
With
hydrogenchloride; ammonium acetate; N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N,N-tetramethyluroniumhexafluorophosphate;
In
1,4-dioxane; o-xylene; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.10.057
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride / 1,4-dioxane / 20 °C
2: O-(benzotriazol-1-yl)-N,N,N,N-tetramethyluroniumhexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C
With
hydrogenchloride; N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N,N-tetramethyluroniumhexafluorophosphate;
In
1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.10.057
