dichloro[(η⁶-p-cymene)(2,2',2''-(10-(2-((2-(4-(diphenylphosphino)benzamido)ethyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetic acid)ruthenium(II)]

Base Information

• Chemical Name: dichloro[(η⁶-p-cymene)(2,2',2''-(10-(2-((2-(4-(diphenylphosphino)benzamido)ethyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetic acid)ruthenium(II)]
• CAS No.: 1618093-97-2
• Molecular Formula: C₄₇H₆₁Cl₂N₆O₈PRu
• Molecular Weight: 1040.99

Synonyms:

Chemical Property of dichloro[(η⁶-p-cymene)(2,2',2''-(10-(2-((2-(4-(diphenylphosphino)benzamido)ethyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetic acid)ruthenium(II)]

Chemical Property:

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Technology Process of dichloro[(η⁶-p-cymene)(2,2',2''-(10-(2-((2-(4-(diphenylphosphino)benzamido)ethyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetic acid)ruthenium(II)]

There total 1 articles about dichloro[(η⁶-p-cymene)(2,2',2''-(10-(2-((2-(4-(diphenylphosphino)benzamido)ethyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetic acid)ruthenium(II)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

[RhCl2(p-cymene)]2 + 2,2',2''-(10-(2-((2-(4-(diphenylphosphino)benzamido)ethyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetic acid (1618093-96-1) → dichloro[(η6-p-cymene)(2,2',2''-(10-(2-((2-(4-(diphenylphosphino)benzamido)ethyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetic acid)ruthenium(II)] (1618093-97-2)

Guidance literature:

In dichloromethane; at 20 ℃; for 19h; Inert atmosphere;

DOI:10.1002/cmdc.201300494

Reference yield: 73.0%

dichloro[(η6-p-cymene)(2,2',2''-(10-(2-((2-(4-(diphenylphosphino)benzamido)ethyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetic acid)ruthenium(II)] (1618093-97-2) + samarium(III) trifluoromethanesulfonate → dichloro[(η6-p-cymene)(samarium 2,2',2''-(10-(2-((2-(4-(diphenylphosphino)benzamido)ethyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetate)ruthenium(II)]

Guidance literature:

In acetonitrile; at 20 ℃; for 36h;

DOI:10.1002/cmdc.201300494

Reference yield:

(153)Sm + dichloro[(η6-p-cymene)(2,2',2''-(10-(2-((2-(4-(diphenylphosphino)benzamido)ethyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetic acid)ruthenium(II)] (1618093-97-2) → C47H58Cl2N6O8PRu(153)Sm

Guidance literature:

In water; at 70 ℃; for 0.166667h; pH=Ca. 5.5;

DOI:10.1002/cmdc.201300494

upstream raw materials:

2,2',2''-(10-(2-((2-(4-(diphenylphosphino)benzamido)ethyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetic acid

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