C₁₄H₁₆O₅

Base Information

Chemical Name:C₁₄H₁₆O₅
CAS No.:1279711-72-6
Molecular Formula:C₁₄H₁₆O₅
Molecular Weight:264.278
Hs Code.:

C<sub>14</sub>H<sub>16</sub>O<sub>5</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₆O₅

Chemical Property:

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Technology Process of C₁₄H₁₆O₅

There total 4 articles about C₁₄H₁₆O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1279711-39-5
3-deoxy-4,6-O-p-methoxybenzylidene-D-galactal

: C₁₄H₁₆O₅

: 1279711-72-6
C₁₄H₁₆O₅

Guidance literature:: With 3,3-dimethyldioxirane; In dichloromethane; at -55 ℃; for 48h; optical yield given as %de; stereoselective reaction;
DOI:10.1021/jo102382r

Reference yield:

: 1279711-37-3
C₂₇H₂₈O₆S

: C₁₄H₁₆O₅

: 1279711-72-6
C₁₄H₁₆O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.75 h / 0 - 20 °C

1.2: 16 h / 20 °C

2.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 0.5 h / Reflux

3.1: lithium 1-naphthalenide / tetrahydrofuran / -40 °C

4.1: 3,3-dimethyldioxirane / dichloromethane / 48 h / -55 °C

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; 3,3-dimethyldioxirane; sodium hydride; lithium 1-naphthalenide; In tetrahydrofuran; dichloromethane; toluene; mineral oil;
DOI:10.1021/jo102382r

Reference yield:

: 1315305-92-0
C₂₉H₃₀O₆S₃

: C₁₄H₁₆O₅

: 1279711-72-6
C₁₄H₁₆O₅

Guidance literature:: Multi-step reaction with 3 steps

1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 0.5 h / Reflux

2: lithium 1-naphthalenide / tetrahydrofuran / -40 °C

3: 3,3-dimethyldioxirane / dichloromethane / 48 h / -55 °C

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; 3,3-dimethyldioxirane; lithium 1-naphthalenide; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/jo102382r